Process method for reducing shrinkage rate of coal gangue-based insulating bricks in roasting process
A process method, the technology of coal gangue, applied in the field of building materials, can solve the problems of easy cracking of products and lower thermal conductivity
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Embodiment 1
[0016] A process method for reducing the shrinkage rate of coal gangue-based insulation bricks in the roasting process, the specific process method is as follows:
[0017] 1) Put the weighed shrimp shells in a crusher and rotate them for 2 minutes, put the shrimp shell powder in 1M hydrochloric acid solution and stir at 500r / min for 2 hours, wash the reacted suspension with distilled water until it is neutral, and remove the suspension Minerals in the solution, then placed in 1M sodium hydroxide solution, stirred at 500r / min in an oil bath at 80°C for 1h, washed the reacted suspension with distilled water until neutral, removed the protein in the suspension, and then placed Bleach in a sodium chlorite solution with a mass concentration of 0.2% for 1 hour, wash the product with distilled water, dry it, and then immerse it in a sodium hydroxide solution with a sodium borohydride content of 0.04%, and the sodium hydroxide solution has a mass percentage of 30% %, placed in an oil ...
Embodiment 2
[0030] A process method for reducing the shrinkage rate of coal gangue-based insulation bricks in the roasting process, the specific process method is as follows:
[0031] 1) Put the weighed shrimp shells in a crusher and rotate them for 2 minutes, put the shrimp shell powder in a 1.5M hydrochloric acid solution and stir at 550r / min for 2.5 hours, wash the reacted suspension with distilled water until it is neutral, remove Minerals in the suspension, then placed in 1.3M sodium hydroxide solution, stirred at 550r / min for 1.5h under an oil bath at 85°C, washed the reacted suspension with distilled water until it was neutral, and removed the minerals in the suspension. The protein is then bleached in a sodium chlorite solution with a mass concentration of 0.3% for 1.5h, the product is washed with distilled water and dried, and then immersed in a sodium hydroxide solution with a sodium borohydride content of 0.05%. The mass percentage of the solution is 32%, put it in a 90°C oil b...
Embodiment 3
[0044] A process method for reducing the shrinkage rate of coal gangue-based insulation bricks in the roasting process, the specific process method is as follows:
[0045] 1) Put the weighed shrimp shells in a crusher and rotate them for 3 minutes, put the shrimp shell powder in a 2M hydrochloric acid solution and stir at 600r / min for 3 hours, wash the reacted suspension with distilled water until it is neutral, and remove the suspension Minerals in 1.5M sodium hydroxide solution, stirred at 600r / min under 90°C oil bath for 2h, washed the reacted suspension with distilled water until neutral, removed the protein in the suspension, and then Place in a sodium chlorite solution with a mass concentration of 0.4% for bleaching for 2 hours, wash the product with distilled water, dry it, and then immerse it in a sodium hydroxide solution with a sodium borohydride content of 0.07%. The mass percentage of the sodium hydroxide solution is 35%, put it in a 95°C oil bath, stir at 600r / min...
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