Process method for reducing shrinkage rate of coal gangue-based insulating bricks in roasting process

A process method, the technology of coal gangue, applied in the field of building materials, can solve the problems of easy cracking of products and lower thermal conductivity

Inactive Publication Date: 2020-08-18
蚌埠创特新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During the firing process of insulation bricks, various chemical components on the surface and inside of insulation bricks liquefy under the action of high temperature to form a liquid phase, which moves inside the insulation bricks under its own gravity, liquid phase surface tension and capillary action, and begins to Encapsulate solid powder particles and expanded perlite and generate new crystal phases. With the increasing liquid phase formation, the crystal phase grows completely, and the expanded perlit...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] A process method for reducing the shrinkage rate of coal gangue-based insulation bricks in the roasting process, the specific process method is as follows:

[0017] 1) Put the weighed shrimp shells in a crusher and rotate them for 2 minutes, put the shrimp shell powder in 1M hydrochloric acid solution and stir at 500r / min for 2 hours, wash the reacted suspension with distilled water until it is neutral, and remove the suspension Minerals in the solution, then placed in 1M sodium hydroxide solution, stirred at 500r / min in an oil bath at 80°C for 1h, washed the reacted suspension with distilled water until neutral, removed the protein in the suspension, and then placed Bleach in a sodium chlorite solution with a mass concentration of 0.2% for 1 hour, wash the product with distilled water, dry it, and then immerse it in a sodium hydroxide solution with a sodium borohydride content of 0.04%, and the sodium hydroxide solution has a mass percentage of 30% %, placed in an oil ...

Embodiment 2

[0030] A process method for reducing the shrinkage rate of coal gangue-based insulation bricks in the roasting process, the specific process method is as follows:

[0031] 1) Put the weighed shrimp shells in a crusher and rotate them for 2 minutes, put the shrimp shell powder in a 1.5M hydrochloric acid solution and stir at 550r / min for 2.5 hours, wash the reacted suspension with distilled water until it is neutral, remove Minerals in the suspension, then placed in 1.3M sodium hydroxide solution, stirred at 550r / min for 1.5h under an oil bath at 85°C, washed the reacted suspension with distilled water until it was neutral, and removed the minerals in the suspension. The protein is then bleached in a sodium chlorite solution with a mass concentration of 0.3% for 1.5h, the product is washed with distilled water and dried, and then immersed in a sodium hydroxide solution with a sodium borohydride content of 0.05%. The mass percentage of the solution is 32%, put it in a 90°C oil b...

Embodiment 3

[0044] A process method for reducing the shrinkage rate of coal gangue-based insulation bricks in the roasting process, the specific process method is as follows:

[0045] 1) Put the weighed shrimp shells in a crusher and rotate them for 3 minutes, put the shrimp shell powder in a 2M hydrochloric acid solution and stir at 600r / min for 3 hours, wash the reacted suspension with distilled water until it is neutral, and remove the suspension Minerals in 1.5M sodium hydroxide solution, stirred at 600r / min under 90°C oil bath for 2h, washed the reacted suspension with distilled water until neutral, removed the protein in the suspension, and then Place in a sodium chlorite solution with a mass concentration of 0.4% for bleaching for 2 hours, wash the product with distilled water, dry it, and then immerse it in a sodium hydroxide solution with a sodium borohydride content of 0.07%. The mass percentage of the sodium hydroxide solution is 35%, put it in a 95°C oil bath, stir at 600r / min...

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Abstract

The invention discloses a technological method for reducing the shrinkage rate of coal gangue-based insulating bricks in a roasting process, and relates to the technical field of building materials. The technological method specifically comprises the following steps of: 1) preparing a nano chitin dispersion liquid from shrimp shells; 2) adding multiwalled carbon nanotubes into a nanocellulose suspension, and adding alumina fibers and mullite fibers to obtain a fiber dispersion liquid; 3) uniformly mixing aluminum oxide sol and silicon dioxide sol to obtain composite sol; and 4) uniformly mixing the products obtained in the steps 1) and 2), drying an obtained mixture to obtain composite fibers, drying and screening coal gangue, fly ash and engineering spoil, adding water, adding the composite fibers and the composite sol, performing aging, adding expanded perlite, and carrying out compression molding, drying, and roasting. According to the production process provided by the invention, the volume shrinkage rate of the insulating bricks can be effectively reduced, and the deformation of the insulating bricks is reduced, so that the insulating bricks are not easy to crack in a high-temperature roasting process, and the performance of the insulating bricks is improved.

Description

technical field [0001] The invention belongs to the technical field of building materials, and in particular relates to a process for reducing the shrinkage rate of coal gangue-based thermal insulation bricks during the roasting process. Background technique [0002] With the continuous development and progress of society, people have higher and higher requirements for the use and function of buildings, and building energy consumption has received great attention. Studies have shown that in the total heat loss of a building, the heat lost through the outer wall accounts for 35-49%, so new thermal insulation materials with good thermal insulation performance are the development trend of the construction industry. Coal gangue is a kind of solid waste produced in the process of coal mining and coal washing. According to incomplete statistics, the cumulative stacking volume of coal gangue has reached more than 5 billion tons, and the annual discharge is increasing by 100 million...

Claims

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Application Information

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IPC IPC(8): C04B33/36C04B33/135C04B33/132C04B33/13
CPCC04B33/13C04B33/132C04B33/1352C04B33/36C04B2235/6562C04B2235/6567C04B2235/96C04B2235/9607Y02P40/60
Inventor 郭艳
Owner 蚌埠创特新材料科技有限公司
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