Expandable selective long-acting water plugging agent and preparation method thereof
A water-blocking agent and selective technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of weak corrosion resistance and scourability, short validity period of water-blocking agent, poor salt resistance of water-blocking agent, etc. , to achieve the effect of temperature resistance and salt resistance adsorption performance, long water blocking validity period and high blocking strength
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Embodiment 1
[0024] A preparation method of an expandable selective long-acting water blocking agent, comprising the steps of:
[0025] Step 1, prepare polyurethane prepolymer: take by weighing 30 grams of polyethylene glycol (moisture removal in advance), 20 grams of polytetrahydrofuran diol (moisture removal in advance) and put them into a three-necked flask, add 30 grams of toluene diisocyanate (preliminary removal of water) under stirring Remove water), heat up to 80°C, react for 2h, and vacuum degas at 80°C for 0.5h to obtain the polyurethane prepolymer. Weigh 70g of the polyurethane prepolymer, which is the A component.
[0026] Step 2. Preparation of functional liquid: 6 grams of acrylamide, 2 grams of 2-acrylamide-2-methylpropanesulfonic acid, 0.01 grams of azobisisobutylimidazoline, 2 grams of hydrophilic nano-silica, 0.05 1 g of triethanolamine and 3 g of trimethylolpropane were sequentially added into 16.94 g of water and stirred evenly to obtain component B.
[0027] Step 3. P...
Embodiment 2
[0030] A preparation method of an expandable selective long-acting water blocking agent, comprising the steps of:
[0031] Step 1, prepare polyurethane prepolymer: take by weighing 25 grams of polycaprolactone diol (removal of moisture in advance), 35 grams of polycarbonate diol (removal of moisture in advance) and put into a three-necked flask, add 30 grams of 1 under stirring, 6-hexamethylene diisocyanate, heated up to 80°C, reacted for 2h, degassed in vacuum at 80°C for 0.5h to obtain a polyurethane prepolymer, weighed 80 grams of polyurethane prepolymer, which was the A component.
[0032] Step 2. Preparation of functional liquid: 4 grams of acrylamide, 1 gram of acrylic acid, 2 grams of nano-aluminum oxide, 0.01 gram of ammonium persulfate, 0.01 gram of sodium bisulfite, 0.03 gram of dibutyltin dilaurate, 3 grams of three Isopropanolamine was sequentially added into 9.95 g of water and stirred evenly to obtain component B.
[0033] Step 3. Pour component A and component ...
Embodiment 3
[0036] A preparation method of an expandable selective long-acting water blocking agent, comprising the steps of:
[0037] Step 1. Preparation of polyurethane prepolymer: Weigh 50 grams of polytetramethylene ether glycol (remove moisture in advance), put it into a three-necked flask, add 40 grams of methylcyclohexyl diisocyanate under stirring, and heat up to 80°C. React for 2 hours, and vacuum degas at 80° C. for 0.5 hours to obtain a polyurethane prepolymer. Weigh 60 grams of the polyurethane prepolymer, which is component A.
[0038] Step 2. Preparation of functional liquid: 12 grams of acrylamide, 2 grams of 2-acrylamide-2-methylpropanesulfonic acid, 1 gram of acrylic acid, 5 grams of nano-calcium carbonate, 0.05 grams of ammonium persulfate, 1 gram of stannous octoate , 2 grams of 1,4-butanediol were added to 16.95 grams of water in turn, and stirred evenly to obtain component B.
[0039] Step 3. Pour component A and component B liquids into the reactor and stir evenly, ...
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