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A kind of ceramic matrix composite material component with stepped structure and preparation method thereof

A composite material component and ceramic matrix technology, which is applied in the field of ceramic matrix composite material components with a stepped structure and their preparation, can solve the problems of high failure rate and high production cost, and achieve increased bonding force, reduced production cost, The effect of reducing the number of machining operations

Active Publication Date: 2022-07-19
GONG YI VAN-RES INNOVATION COMPOSITE MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In order to overcome the problems of high failure rate and high production cost caused by delamination, cracks, deformation and fracture at the step joints of ceramic matrix composite components with stepped structures in the prior art, the purpose of the present invention is to provide A ceramic matrix composite material component with a stepped structure and a preparation method thereof, which improve the overall strength of the component and the strength of the junction of the stepped structure, thereby increasing the qualified rate of products and reducing production costs

Method used

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  • A kind of ceramic matrix composite material component with stepped structure and preparation method thereof

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Effect test

Embodiment 1

[0037] A ceramic matrix composite component with a step structure, which is composed of a fiber preform, an interface layer and a ceramic matrix deposited on the fiber preform in turn; including a base part and a step structure part arranged on the base part; the base Parts are integrally formed with the fiber preform of the step structure part; the fiber preform as a whole is made of 12k carbon fiber, 0 / 90° non-woven fabric laminate / mesh layup needle punched 2.5D preform, and the step structure part of the fiber The fiber density of the preform gradually decreases from the inside to the outside; the layer ratio of the 0 / 90° laminated non-woven fabric / mesh tire inside the stepped structure part of the preform is 6:1, and the layers of the non-woven fabric and the mesh tire are not layered from the inside to the outside. The number ratio is gradually reduced to 2:1; the interface layer is a pyrolytic carbon interface layer; the ceramic matrix of the base part is silicon carbide;...

Embodiment 2

[0062] A ceramic matrix composite component with a step structure, which is composed of a fiber preform, an interface layer and a ceramic matrix deposited on the fiber preform in turn; including a base part and a step structure part arranged on the base part; the base Part of the fiber preform of the step structure part is integrally formed; the fiber preform is made of 12K carbon fiber as a whole, and the 2.5D preform is formed by fine weaving and puncture; the fiber preform of the step structure part is finely woven from the inside to the outside. The density of the fiber cloth gradually decreases Small, the density of the inner fine woven fiber cloth is 0.70g / cm 3 , the density of the outer fine braided fiber is 0.5g / cm 3 The interface layer is a pyrolytic carbon interface layer; the ceramic matrix of the basic part is a silicon carbide matrix; the ceramic matrix of the step structure part is a silicon carbide matrix containing nanofibers, and the nanofibers are nanofibers....

Embodiment 3

[0083] A ceramic matrix composite component with a stepped structure, which is composed of a fiber preform, an interface layer and a ceramic matrix deposited on the fiber preform in sequence; it includes a base part and a stepped structure part arranged on the base part; the base Part and the fiber preform of the step structure part are integrally formed; the fiber preform is made of 12K silicon carbide fiber as a whole, and the fiber is punctured to form a 2.5D preform; the fiber density of the step structure part of the fiber preform is finely woven from the inside to the outside. The cloth density gradually decreases, and the inner fiber cloth density is 0.60g / cm 3 , the outer fiber density is 0.40g / cm 3 The interface layer is a pyrolytic carbon interface layer; the ceramic matrix of the basic part is a silicon carbide matrix, and the ceramic matrix of the step structure part is a silicon carbide matrix containing nanofibers, and the nanofibers are nanofibers and graphite. ...

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Abstract

The invention discloses a ceramic matrix composite material component with a stepped structure and a preparation method thereof. (1) Processing a fiber preform according to the designed size; (2) preparing an interface layer; (3) partially impregnating the stepped structure of the fiber preform The resin mixed with fibers is then dried; (4) the steps of dipping-curing-low temperature cracking are repeated 2-4 times for the step structure part, and the ceramic precursor slurry containing nanofibers is dipped; (5) the whole dipping-curing-low temperature The cracking is repeated 3-6 times, and the dipping-curing-high temperature cracking step is repeated 1-3 times, and the ceramic precursor slurry containing the nano-ceramic powder is dipped; (6) mechanical finishing; (7) repeat the dipping in step (5) ‑curing‑low temperature cracking step 2~3 times; (8) repeat the dipping‑curing‑high temperature cracking step in step (5) 1~2 times; (9) CVD method to deposit the SiC coating. The invention can improve the strength of the joint of the step structure, thereby improving the product qualification rate and reducing the production cost.

Description

technical field [0001] The invention belongs to the technical field of ceramic matrix composite materials, in particular to a ceramic matrix composite material component with a stepped structure and a preparation method thereof. Background technique [0002] Continuous fiber reinforced ceramic matrix composites have both excellent properties of ceramic matrix and continuous fibers, with high wear resistance, high temperature resistance, corrosion resistance, radiation resistance, high specific strength, low density, small thermal expansion coefficient, ablation resistance, oxidation resistance, etc. Excellent performance, as a high-temperature thermal structural material and wear-resistant material, it is expected to be used in aero-engines, space stations, automobile brake discs, nuclear power and other fields. [0003] With the development of science and technology, the use environment of continuous fiber reinforced ceramic matrix composites is more complex, and the struct...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/80C04B35/571
CPCC04B35/571C04B2235/5248C04B2235/3826C04B2235/602C04B2235/656C04B2235/6562C04B2235/6567C04B2235/6581C04B2235/77C04B2235/96
Inventor 吴恒魏庆渤张东生马美霞曹伟李江涛刘毫毫胡晓辉王琰董会娜
Owner GONG YI VAN-RES INNOVATION COMPOSITE MATERIAL CO LTD