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A kind of preparation method of indium phosphide substrate

A technology of indium phosphide and substrate, applied in the field of indium phosphide substrate preparation, can solve the problems of shortening the CMP polishing time of indium phosphide substrate, environmental pollution, health and safety hazards, etc., to shorten the CMP polishing time and improve corrosion The effect of improving efficiency and effective life

Active Publication Date: 2022-02-22
中锗科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The invention provides a method for preparing an indium phosphide substrate. The front and back sides of the wafer are respectively processed by grinding and thinning, and the main surface with a roughness Ra value of 100-150 nm can be obtained before the wafer is subjected to CMP polishing. materials, greatly reducing the thickness of the damaged layer of the substrate before polishing, and greatly shortening the CMP polishing time of the indium phosphide substrate; A series of problems such as high mechanical damage rate on the bottom surface, thick mechanical damage layer, poor surface roughness, and poor flatness consistency; through the improvement and optimization of the composition of the corrosion solution, it has solved the problems of hydrochloric acid, glacial acetic acid, bromine and other acids in the corrosion solution in the past. During the operation process, the environmental pollution caused by volatilization and the health and safety hazards brought to the operators, at the same time, the effective life of the new component corrosive solution has been greatly improved.

Method used

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  • A kind of preparation method of indium phosphide substrate
  • A kind of preparation method of indium phosphide substrate
  • A kind of preparation method of indium phosphide substrate

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Experimental program
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Embodiment 1

[0031] The preparation method of indium phosphide substrate, comprises the steps:

[0032] 1) Use a multi-wire cutting machine to cut out a 4-inch indium phosphide-doped sulfur wafer with a thickness of 700um, such as figure 2 As shown, and the edge of the wafer is ground and chamfered, so that the longitudinal section of the edge of the wafer is arc-shaped, as shown in image 3 shown;

[0033] 2) Use a grinding machine to grind the back of the wafer obtained in step 1) to remove the saw lines caused by multi-wire cutting on the back. When grinding, the pressure per unit area of ​​the wafer is 0.5N / cm 2 , no scratches on the surface;

[0034] 3) On the thinning machine, the wafer obtained in step 2) is first thinned on the front side and then thinned on the back side, using diamond grinding wheels of 2000# (3-8 microns in particle size) and 8000# (<1 micron in particle size) respectively Grinding the wafer, the grinding speed is 1300rpm, so that the wafer is uniformly thin...

Embodiment 2

[0056] The preparation method of indium phosphide substrate, comprises the steps:

[0057] 1) Use a multi-wire cutting machine to cut out a 2-inch indium phosphide sulfur-doped wafer with a thickness of 400um, such as figure 2 As shown, and the edge of the wafer is ground and chamfered, so that the longitudinal section of the edge of the wafer is arc-shaped, as shown in image 3 shown;

[0058] 2) Use a grinding machine to grind the back of the wafer obtained in step 1) to remove the saw lines caused by multi-wire cutting on the back. When grinding, the pressure per unit area of ​​the wafer is 0.25N / cm 2 ;

[0059] 3) On the thinning machine, the front side of the wafer obtained in step 2) is thinned, and the diamond grinding wheel of 2000# (particle diameter 3-8 micron) and 8000# (particle diameter<1 micron) is used respectively to grind the wafer, and the grinding The rotation speed is 1300rpm, so that the wafer is uniformly thinned, and at the same time, an ultra-fine s...

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Abstract

The invention discloses a preparation method of an indium phosphide substrate, which sequentially includes the steps of cutting, back grinding, front thinning, corrosion, polishing, cleaning and packaging. The preparation method of the indium phosphide substrate of the present invention creatively develops a method of combining grinding and thinning to process the front and back sides of the wafer respectively, and can obtain a roughness Ra value of 100-150nm before the wafer is subjected to CMP polishing. The incoming material on the main surface greatly reduces the thickness of the damaged layer of the substrate before polishing, and greatly shortens the CMP polishing time of the indium phosphide substrate; A series of problems such as high mechanical damage rate on the substrate surface, mechanical damage layer thickness, poor surface roughness, and poor flatness consistency; through the improvement of the corrosion solution, environmental pollution is reduced, the working environment is improved, and the effective life of the corrosion solution is extended. It has been greatly improved, and the corrosion efficiency has been improved at the same time.

Description

technical field [0001] The invention relates to a method for preparing an indium phosphide substrate, belonging to the technical field of indium phosphide substrate preparation. Background technique [0002] Indium phosphide (InP) is a second-generation semiconductor material with a zinc blende crystal structure and a band gap of 1.34eV. It is used as a substrate material for optoelectronic chips with high electron mobility, high band gap, and high thermal conductivity. It is the key material of optical module semiconductor laser and receiver. According to the semiconductor LD and LED, the flatness of the substrate has a decisive influence on the formation of the epitaxial film and when it is made into a device. [0003] According to the status quo in the industry, the current processing of indium phosphide substrates is double-sided grinding, and a considerable part of the wafer thickness needs to be removed during the processing, resulting in waste of crystal materials, a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01L21/02
CPCH01L21/02016H01L21/02013H01L21/02021H01L21/02019H01L21/02052
Inventor 刘兴达周锐柯尊斌吴怀东
Owner 中锗科技有限公司
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