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Alloy treatment method based on plasma immersion ion implantation

A technology of immersion ion implantation and plasma, which is applied in the field of biomedical materials, can solve the problem of affecting the thickness uniformity and bonding strength of the micro-arc oxidation coating, the insufficient bonding strength of the implant and the host bone tissue, and the excessive growth of the local oxide film To achieve uniform surface modification effect, improve thickness uniformity and bonding strength, and improve safety hazards

Pending Publication Date: 2022-05-03
安徽中科大禹科技有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] There are still some problems in the method of micro-arc discharge on the surface of titanium alloy to prepare nano-bionic structures. Although titanium alloy has good biocompatibility, it is completely different from natural bone in composition and structure, and is still an inert biomaterial. After the body, it will be covered by a layer of encapsulating fibrous membrane, which cannot form a chemical bond with the bone tissue. It is only a mechanical chimera, which will easily lead to insufficient bonding strength between the implant and the host bone tissue, and the wound will not heal after surgery. and other issues, this method does not treat the titanium alloy material; in the process of putting the titanium alloy into the electrolyte, the conventional micro-arc discharge method is adopted, and the method has not been improved. The concentration at the interface between the metal and the electrolyte solution If the gradient is large, there may be uneven current distribution and excessive growth of local oxide film, which will affect the thickness uniformity and bonding strength of the micro-arc oxidation coating.

Method used

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  • Alloy treatment method based on plasma immersion ion implantation
  • Alloy treatment method based on plasma immersion ion implantation
  • Alloy treatment method based on plasma immersion ion implantation

Examples

Experimental program
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Embodiment 1

[0057] Such as Figure 1 to Figure 4 As shown, the metal three-dimensional printing equipment used in this method includes a main body 1, a working cabin 101 and a smoke exhaust hole 102 are arranged inside the main body 1, and a support 2 and a filter box are installed on the outside of the main body 1 3. The inside of the support 2 is provided with a high-temperature passage connected with the filter box 3, and the high-temperature passage communicates with the smoke exhaust hole 102 through the intake pipe 4. The filter box 3 is provided with an air outlet pipe 5, and the inside of the filter box 3 is installed with a pair of The first-stage filter element 301 and the second-stage filter element 302 for filtering and purifying the smog, the main body 1 is equipped with an air extractor connected with the air outlet pipe 5 . When working, the metal three-dimensional printing equipment will generate high-temperature smoke inside the working cabin 101 during the working proces...

Embodiment 2

[0064] Such as Figure 7 As shown in Comparative Example 1, another embodiment of the present invention is: a compression spring is installed on the active rod 15, a boss is provided on the end of the driven rod 16 close to the active rod 15, and the active rod 15 is movably inserted Connected to the inside of the boss, the inside of the boss is provided with a chute corresponding to the active rod 15, and the active rod 15 is provided with a hook for hooking the driven rod 16, and there is a gap between the hook and the groove bottom of the chute. There is a gap, the inside of the top seat 14 is movably plugged with a clamping plate 20 for clamping the boss, a back-moving spring is installed on the clamping plate 20, and a push plate 21 for pushing away the clamping plate 20 is fixedly installed on the active rod 15. The plate 21 is provided with a slope, the inside of the clamping plate 20 is provided with a through groove corresponding to the push plate 21 , and the bottom ...

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Abstract

The invention belongs to the field of biomedical materials, and particularly relates to an alloy treatment method based on plasma immersion ion implantation, which comprises the following steps: preparing a porous titanium alloy material with a porous structure; an ultrasonic auxiliary device is loaded, and the titanium alloy material is treated through a micro-plasma oxidation method; carrying out surface functional modification on the titanium alloy material by adopting a plasma immersion ion implantation technology; constructing a bionic titanium alloy material with multiple surface functions; the strength and modulus of the porous titanium alloy can be changed through a method of introducing gaps into the titanium alloy, the mechanical property of the material is effectively regulated and controlled, the mechanical behavior of the material is improved, the material is better matched with surrounding bone tissues, and the titanium alloy material is further subjected to surface functional modification through a plasma immersion ion implantation technology, so that the mechanical property of the material is improved. The modification depth is large, the treatment effect is lasting, the surface modification effect is uniform, and application requirements are closer.

Description

technical field [0001] The invention belongs to the field of biomedical materials, in particular to an alloy treatment method based on plasma immersion ion implantation. Background technique [0002] Titanium and its alloys have many advantages in the application of orthopedic implant materials, such as low density, high strength, good toughness, good biocompatibility, non-toxic, low elastic modulus, good corrosion resistance, low X-ray absorption rate etc., thus occupying an increasingly important position in orthopedic metal materials, and the construction of bionic titanium alloys to replace traditional dense titanium alloys is the development trend of medical titanium alloy implant materials. [0003] A Chinese patent with the publication number CN106282907A discloses a method for preparing a nano-bionic structure by micro-arc discharge on the surface of a titanium alloy, including the following steps: S1, preparing electrolyte; S2, preparing a nano-bionic structure by m...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F10/62B22F10/28C25D11/26C25D5/20C23C14/48B33Y10/00B33Y30/00B33Y40/20B22F12/00B22F12/70B22F10/77C22C1/08B01D46/62B01D46/76B01D46/10
CPCB22F10/62B22F10/28C25D11/026C25D11/26C25D5/20C23C14/48B33Y10/00B33Y30/00B33Y40/20B22F12/00B22F12/70B22F10/77A61L27/06A61L27/30A61L27/56A61L31/022A61L31/082A61L31/146B01D46/10B01D46/0036A61L2400/18A61L2420/02
Inventor 吴征威汤祺周海晨
Owner 安徽中科大禹科技有限公司