Waterborne polyurethane PE/POE (Polyethylene/Polyolefin Elastomer) composite waterproof coiled material as well as preparation method and application thereof
A water-based polyurethane and waterproof membrane technology, which is applied in polyurea/polyurethane adhesives, modified epoxy resin adhesives, roofs using flexible materials, etc., can solve the problems of brittle cracks, PE/POE composite materials Flammability needs to be improved, easy to flow and other problems, to achieve good flame retardancy, improve flame retardancy and mechanical strength and mechanical properties, and improve the effect of bonding strength
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Embodiment 1
[0040] A preparation method of water-based polyurethane PE / POE composite waterproofing membrane, comprising the following steps:
[0041] S1: Preparation of PE / POE composite film base:
[0042] a. Prepare materials according to the following weights: 50 parts of polyethylene, 10 parts of ethylene-octene copolymer, 15 parts of polystyrene, 20 parts of polyurethane prepolymer, 15 parts of ethyl 2-hydroxymethyl acrylate, dibutyltin dilaurin 0.5 part of acid ester, 1 part of benzoyl peroxide, 10 parts of reactive flame retardant;
[0043]The reactive flame retardant is prepared by mixing pentaerythritol phosphate melamine salt and N,N-bis(2-hydroxyethyl)aminomethylenephosphonate diethyl ester in a mass ratio of 1.5:1;
[0044] b. Pre-dry polyethylene and ethylene-octene copolymer in an oven at 60°C for 24h;
[0045] c. Add polyethylene, ethylene-octene copolymer and polystyrene, polyurethane prepolymer, 2-hydroxymethyl ethyl acrylate, dibutyltin dilaurate, benzoyl peroxide, reac...
Embodiment 2
[0052] A preparation method of water-based polyurethane PE / POE composite waterproofing membrane, comprising the following steps:
[0053] S1: Preparation of PE / POE composite film base:
[0054] a. Prepare materials according to the following mass parts: 70 parts of polyethylene, 30 parts of ethylene-octene copolymer, 17.5 parts of polystyrene, 25 parts of polyurethane prepolymer, 17.5 parts of ethyl 2-hydroxymethacrylate, 0.75 parts of stannous octoate parts, 1.5 parts of diisopropyl peroxydicarbonate, and 12.5 parts of reactive flame retardant;
[0055] The reactive flame retardant is prepared by mixing pentaerythritol phosphate melamine salt and N,N-bis(2-hydroxyethyl)aminomethylenephosphonic acid diethyl ester in a mass ratio of 2:1;
[0056] b. Pre-dry polyethylene and ethylene-octene copolymer in an oven at 60°C for 24h;
[0057] c. Add polyethylene, ethylene-octene copolymer and polystyrene, polyurethane prepolymer, ethyl 2-hydroxymethyl acrylate, stannous octoate, dii...
Embodiment 3
[0064] A preparation method of water-based polyurethane PE / POE composite waterproofing membrane, comprising the following steps:
[0065] S1: Preparation of PE / POE composite film base:
[0066] a. Prepare materials according to the following weights: 90 parts of polyethylene, 50 parts of ethylene-octene copolymer, 20 parts of polystyrene, 30 parts of polyurethane prepolymer, 20 parts of ethyl 2-hydroxymethyl acrylate, dibutyltin diacetate 1 part, 1.5 parts of dicumyl peroxide, 15 parts of reactive flame retardant;
[0067] The reactive flame retardant is prepared by mixing pentaerythritol phosphate melamine salt and N,N-bis(2-hydroxyethyl)aminomethylenephosphonic acid diethyl ester in a mass ratio of 3:1;
[0068] b. Pre-dry polyethylene and ethylene-octene copolymer in an oven at 60°C for 24h;
[0069] c. Add polyethylene, ethylene-octene copolymer and polystyrene, polyurethane prepolymer, 2-hydroxymethyl ethyl acrylate, dibutyltin diacetate, dicumyl peroxide, and reactive ...
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