Equipment and process for osmosizing and plating metal carboritride by dual-glow discharge
A technology of nitrogen compound and permeation plating, which is applied in the direction of metal material coating process, coating, solid-state diffusion coating, etc., can solve the problems of few applications, expensive equipment, and high cost
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[0016] Take metal nitride TaN as an example:
[0017] After the vacuum chamber 1 is evacuated to a vacuum degree below 1 Pa by the mechanical pump exhaust system 8, Ar gas and N are supplied by the gas supply system at a ratio of 5:5. 2 Mixed gas with a partial pressure of 20-100Pa, an adjustable metal source power supply 6 is added between the anode 5 and the source 4 made of a grid-shaped tantalum plate, and the voltage is 800-1200V; between the anode 5 and the workpiece 3 Add an adjustable negative bias power supply 7 with a voltage of 400-800V. Make it produce double-layer glow discharge, and use the equipotential hollow cathode effect in the grid-shaped tantalum source and the unequal potential hollow cathode effect between the grid-shaped tantalum source 4 and the workpiece 3 to make the workpiece to be infiltrated 3 Raise to 800-1000°C, and the tantalum atoms and ions sputtered from the grid-shaped tantalum source, and the dissociated N atoms and N ions quickly reach t...
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