Inorganic surface treating method for nano-zinc oxide
A nano-zinc oxide and surface treatment technology, applied in the field of nano-materials, can solve problems such as poor inorganic surface treatment effect, and achieve the effects of easy control, good dispersibility, and improved dispersibility
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0023] Example 1
[0024] The specific implementation is as follows:
[0025] (1) Take 1000 g of nano zinc oxide aqueous dispersion with a mass percentage of 25%, adjust the temperature of the nano zinc oxide aqueous dispersion to 30°C, and add 100 mass to the nano zinc oxide aqueous dispersion while stirring. 5% aluminum chloride (AlCl 3 ) An aqueous solution and a sodium phosphate aqueous solution with a mass percentage of 3%, and the pH of the system is maintained at 8.0, and the co-current feeding time is 30 minutes. The amount of aluminum chloride to generate AlPO 4 In terms of mass, it accounts for 3% of the mass of nano zinc oxide. After the aluminum chloride aqueous solution is added, continue to stir and mature at 30°C for 120 minutes.
[0026] (2) Raise the temperature of the nano-zinc oxide slurry obtained in step (1) to 95°C, while stirring, add a 30% by mass aqueous solution of sodium silicate to the nano-zinc oxide slurry and the amount of sodium silicate To generate...
Example Embodiment
[0028] Example 2
[0029] The specific implementation is as follows:
[0030] (1) Take 1000 g of nano zinc oxide aqueous dispersion with a mass percentage of 25%, adjust the temperature of the nano zinc oxide aqueous dispersion to 90 ℃, while stirring, add 100 mass to the nano zinc oxide aqueous dispersion. 30% aluminum nitrate (Al(NO 3 ) 3 ·9H 2O) An aqueous solution and a sodium phosphate aqueous solution with a mass percentage of 30%, and the pH of the system is maintained at 10.0, and the co-current feeding time is 300 minutes. The amount of aluminum chloride to generate AlPO 4 In terms of mass, it accounts for 10% of the mass of nano zinc oxide. After the aluminum chloride aqueous solution has been added, continue to stir and mature at 90°C for 20 minutes.
[0031] (2) Lower the temperature of the nano-zinc oxide slurry obtained in step (1) to 75°C, while stirring, add 5% by mass potassium silicate aqueous solution to the nano-zinc oxide slurry, the amount of potassium silica...
Example Embodiment
[0033] Example 3
[0034] The specific implementation is as follows:
[0035] (1) Take 1000g of nano zinc oxide aqueous dispersion with a mass percentage of 25%, adjust the temperature of the nano zinc oxide aqueous dispersion to 50°C, and add 100% by mass to the nano zinc oxide aqueous dispersion while stirring. 20% aluminum sulfate (Al 2 (SO 4 ) 3 ·18H 2 O) An aqueous solution and a sodium phosphate aqueous solution with a mass percentage of 10%, and the pH of the system is maintained at 9.0, and the co-current feeding time is 150 minutes. The amount of aluminum chloride to generate AlPO 4 In terms of mass, it accounts for 5% of the mass of nano zinc oxide. After the aluminum sulfate aqueous solution is added, continue to stir and mature at 50°C for 60 minutes.
[0036] (2) Raise the temperature of the nano-zinc oxide slurry obtained in step (1) to 85°C, while stirring, add a 15% sodium silicate aqueous solution with a mass percentage of sodium silicate to the nano-zinc oxide aq...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap