Bacteria and breeding method and method for producing cellulase thereof
A cellulase and cellulose technology, applied in microorganism-based methods, methods using microorganisms, bacteria, etc., can solve problems such as unfavorable separation and purification of cellulase, unfavorable application, and short cycle of bacterial cellulase production.
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Embodiment 1
[0035] Isolation of the cellulose-degrading microorganism Cellulomonas moist from bovine rumen fluid ( Cellulomonas uda ) NJ0807
[0036] 1 Sampling of bovine rumen fluid
[0037] The stomach of buffalo buffalo just slaughtered in a slaughterhouse in Anhui was taken out, the rumen juice was quickly put into a sterile bottle sterilized by high temperature in advance, and the bottle containing the cow rumen juice was quickly transported to the laboratory in a low temperature environment.
[0038] 2 Enrichment culture of cellulose degrading microorganisms
[0039] Cellulose-degrading microorganisms in bovine rumen juice were enriched and cultured in an enriched medium with cellulose as the only carbon source. The composition of the enrichment medium is 0.5% CMC, 0.5% filter paper, 0.2% NaNO 3 , 0.1% K 2 HPO 4 , 0.05% KCl, 0.05% MgSO 4 ·7H 2 O, 0.0001% FeSO 4 , pH natural. The medium was steam sterilized at 121°C for 20 min. Bovine rumen juice was inoculated into a 300mL...
Embodiment 2
[0048] Production of cellulase using the above strains
[0049] The strain Cellulomonas moist ( Cellulomonas uda ) NJ0807 was streak-inoculated into LB solid medium, cultured at 30 °C for 3 days, and then inoculated into liquid seed medium. The composition of the seed medium was 0.5% yeast extract, 0.5% sucrose, 0.4% NaCl, 0.1% K 2 HPO 4 , 0.05% MgSO 4 ·7H 2 O, adjust the initial pH of the medium to 7.5, and sterilize at 121 °C for 20 min. After the bacteria were cultured in the seed medium at 28°C and 180 rpm for 30 hours, the concentration of bacteria accumulated in a large amount, and the seed liquid was inoculated into a 1 L Erlenmeyer flask containing 400 mL of liquid fermentation medium at a 5% (v / v) inoculation amount , the composition of the liquid fermentation medium was 1% peptone, 1% CMC, 0.5% sucrose, 0.4% NaCl, 0.1% K 2 HPO 4 , 0.05% MgSO 4 ·7H 2 O, adjust the initial pH of the medium to 7.5, and sterilize at 121 °C for 20 min. After culturing for 2 days...
Embodiment 3
[0051] Purification of cellulase
[0052] Dissolve the ethanol-precipitated crude enzyme liquid product in an appropriate volume of 20 mM Tris-HCl (pH 8.8) buffer and purify using an anion exchange chromatography Q Sepharose Fast Flow fast protein liquid chromatography (FPLC) purification system using XK 16 Preparative column, ion exchange resin using 20 mmol L -1 Equilibrate with Tris-HCl (pH 8.8) buffer, wash and equilibrate with 10 times column volume of equilibration buffer, add the dissolved crude enzyme solution, the total protein amount loaded is about 10% of the column adsorption capacity. Gradient elution was used for elution, and the NaCl concentration rose to 0.4 mol L within 8 column volumes -1 , with a flow rate of 2 mL min -1 . Collect in different tubes, collect 2 mL in each tube, measure the cellulase activity of the collected parts and combine the active fragments. This purification step resulted in two main cellulase components, in Figure 4 Correspondi...
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