Hydrophilic modification method of polytetrafluoroethylene porous membrane
A technology of polytetrafluoroethylene and hydrophilic modification, which is applied in the field of hydrophilic modification of polytetrafluoroethylene microporous membranes, can solve the problems of unsatisfactory improvement of bonding strength, great harm to human body, and poor surface durability. Improves the effect of hydrophilic treatment, maintains durability, and improves compatibility
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Embodiment 1
[0018] (1) Isophorone diisocyanate is purified by distillation under reduced pressure, and stored in a desiccator for subsequent use;
[0019] (2) Immerse the polytetrafluoroethylene microporous membrane in a solution of fluorine-containing polyether polyol and acetone with a mass fraction of 1:9 for 10 minutes, take it out and dry it in the air to obtain a temporary hydrophilic polytetrafluoroethylene microporous membrane;
[0020] (3) Immerse the temporary hydrophilic polytetrafluoroethylene microporous membrane in the post-treatment solution of dibutyltin dilaurate, isophorone diisocyanate, and acetone with a mass fraction of 0.05:20:79.95, and take it out at 50°C After drying in the air for 1 hour, the unreacted reactive monomers on the membrane were washed away with water, and dried to obtain a permanent hydrophilic polytetrafluoroethylene microporous membrane. The water contact angle of the obtained hydrophilic polytetrafluoroethylene microporous membrane is reduced from...
Embodiment 2
[0023] (1) Toluene-2,4-diisocyanate is purified by vacuum distillation and stored in a desiccator for subsequent use;
[0024] (2) Soak the polytetrafluoroethylene microporous membrane in a solution of fluorine-containing polyether polyol and acetone with a mass fraction of 1:9 for 20 minutes, take it out and dry it in the air to obtain a temporary hydrophilic polytetrafluoroethylene microporous membrane;
[0025] (3) Immerse the temporary hydrophilic polytetrafluoroethylene microporous membrane in the post-treatment solution of stannous octoate, toluene-2,4-diisocyanate, and acetone with a mass fraction of 0.05:20:79.95, and take it out at 30°C After drying in the air for 3 hours, the unreacted reactive monomers on the membrane were washed away with water, and dried to obtain a permanent hydrophilic polytetrafluoroethylene microporous membrane. The water contact angle of the obtained hydrophilic polytetrafluoroethylene microporous membrane is reduced from 130.1 degrees of the...
Embodiment 3
[0028] (1) 4,4-diphenylmethane diisocyanate is purified by vacuum distillation and stored in a desiccator for subsequent use;
[0029] (2) Immerse the polytetrafluoroethylene microporous membrane in the fluorine-containing polyether polyol and acetone solution with a mass fraction of 1:9 for 20 minutes, take it out and dry it in the air to obtain a temporary hydrophilic polytetrafluoroethylene microporous membrane;
[0030] (3) Immerse the temporary hydrophilic polytetrafluoroethylene microporous membrane in the post-treatment solution of dibutyltin dilaurate, toluene-2,4-diisocyanate and acetone with a mass fraction of 0.05:20:79.95, and take it out in After drying in the air at 45°C for 2 hours, wash off the unreacted reactive monomers on the membrane with water, and dry it in the air to obtain a permanent hydrophilic polytetrafluoroethylene microporous membrane. The water contact angle of the obtained hydrophilic polytetrafluoroethylene microporous membrane is reduced from ...
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