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Rana japonica oil polypeptide micro-capsule powder and preparation method thereof

A technology of wood frog oil and microcapsules, which is applied in food preparation, food drying, food science and other directions, can solve the problems of high viscosity of wood frog oil polypeptide solution, easy to absorb moisture and agglomerate, and long dispersion time, so as to shorten the dissolution time, The effect of improving storage stability and solubility

Inactive Publication Date: 2015-03-25
HARBIN MO MEDICAL BIOLOGICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003]However, the Rana oil polypeptide solution processed by enzymolysis still has the problems of high viscosity, difficult concentration, and difficult processing, and because the frog oil raw material itself is very precious, The purification of Rana oil polypeptide will cause a certain degree of waste of raw materials; Rana oil polypeptide itself has bitter and fishy smell, and is easy to oxidize and inconvenient to store. The Rana oil polypeptide powder obtained by direct milling has a large number of hydrophobic groups. Agglomerates, high water content, poor dispersion, easy to absorb moisture and agglomerate, and dissolve in water for a long time; however, there are few related studies on the microencapsulation of Rana oil peptides

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] A wood frog oil polypeptide microcapsule powder and a preparation method thereof, comprising 10-20% of wood frog oil polypeptide core material, 30-50% of maltodextrin, 10-20% of carboxymethyl cellulose sodium, β - Made of 5-20% cyclodextrin and 5-10% porous starch, the Rana oil polypeptide core material is selected, soaked, colloid milled and enzymatically hydrolyzed by papain from dried Rana oil.

[0017] The main steps of its preparation method:

[0018] Step 1. Take the dry wood frog oil, add distilled water with a weight ratio of 1:50-200, soak hair, grind it with a colloid mill, filter it, add ginger juice to remove the fishy smell, and then add 1-5% protease by weight of the dry wood frog oil , kept at 40-50°C for 2-8 hours, cooled after enzymatic hydrolysis to obtain the Rana oil polypeptide core material solution, homogenized, sterilized, and cooled at a temperature of 60-65°C and a pressure of 10-20Mpa To emulsification temperature 60-80 ℃;

[0019] S...

Embodiment 2

[0023] A wood frog oil polypeptide microcapsule powder and a preparation method thereof, comprising 10-20 parts of wood frog oil polypeptide core material, 30-50 parts of maltodextrin, 10-20 parts of carboxymethyl cellulose sodium, Made from 5-20 parts of β-cyclodextrin and 5-10 parts of porous starch.

[0024] The main steps of its preparation method:

[0025] Step 1. Take the dry wood frog oil, add distilled water with a weight ratio of 1:100, soak hair, grind with a colloid mill, filter and add ginger juice to remove the fishy smell, and then add 3% protease by weight of the dry wood frog oil. Incubate at 50°C for 2 hours, enzymatically hydrolyze and cool to obtain the Rana oil polypeptide core material solution, homogenize at 65°C and 20Mpa, sterilize, and cool to emulsification temperature of 80°C;

[0026] Step 2. Select water to dissolve maltodextrin, sodium carboxymethylcellulose, β-cyclodextrin, and porous starch according to weight percentage, and dissolve m...

Embodiment 3

[0030] A wood frog oil polypeptide microcapsule powder and a preparation method thereof, comprising 15 parts of wood frog oil polypeptide core material, 40 parts of maltodextrin, 15 parts of carboxymethyl cellulose sodium, and β-cyclodextrin It is made of 13 parts of essence and 8 parts of porous starch.

[0031] The main steps of its preparation method:

[0032] Step 1. Take the dry wood frog oil, add distilled water with a weight ratio of 1:200, soak hair, grind it with a colloid mill, filter and add ginger juice to remove the fishy smell, and then add 5% protease by weight of the dry wood frog oil. Incubate at 50°C for 2 hours, enzymatically hydrolyze and cool to obtain the Rana oil polypeptide core material solution, homogenize at 60°C and 15Mpa, sterilize, and cool to emulsification temperature of 80°C;

[0033] Step 2. Select water to dissolve maltodextrin, sodium carboxymethylcellulose, β-cyclodextrin, and porous starch according to weight percentage, and disso...

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PUM

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Abstract

The invention discloses a rana japonica oil polypeptide micro-capsule powder and a preparation method thereof. The rana japonica oil polypeptide micro-capsule powder is prepared from the following components by weight percent: 10-20% of rana japonica oil polypeptide core material, 30-50% of maltodextrin, 10-20% of sodium carboxymethyl cellulose, 5-20% of beta-cyclodextrin and 5-10% of porous starch. The rana japonica oil polypeptide core material is prepared by treating a dry product of rana japonica oil in the following steps: selecting, soaking, performing colloid milling and performing enzymolysis by papain. The preparation method of the rana japonica oil polypeptide micro-capsule powder mainly comprises the following steps: 1, preparing a rana japonica oil polypeptide core material solution; 2, mixing solutions; 3, performing treatment of shearing emulsification; 4, performing spray drying and obtaining a finished product. In the preparation method disclosed by the invention, the rana japonica oil polypeptide micro-capsule powder is prepared by using a rana japonica oil polypeptide enzymolysis solution as a raw material and adopting a technology of low-temperature spray drying by appropriate wall material compatibility. The biological activity of polypeptide in the rana japonica oil enzymolysis solution is retained, and many performances of a product are improved. The rana japonica oil polypeptide micro-capsule powder not only can be preserved for a long time as a raw material for further processing, but also can be directly applied as a product, so that a new approach is provided for the deep processing of rana japonica.

Description

technical field [0001] The invention relates to the field of food processing, in particular to a Rana oil polypeptide microcapsule powder and a preparation method thereof. Background technique [0002] Rana oil is the dried fallopian tube of the female Rana, and it is a precious nourishing health product, which has the functions of nourishing the kidney and essence, moistening the lungs and nourishing yin. It is rich in protein, 18 kinds of amino acids, a variety of trace elements and vitamins, especially three sex hormones, namely estradiol, testosterone and progesterone. Rana oil enzymatic hydrolysis solution is to hydrolyze Rana oil through controllable enzyme engineering technology, decompose protein into polypeptides, improve the fluidity and solubility of Rana oil, reduce viscosity, and improve the processing of its industrial production Performance; due to the increase in the content of peptides and amino acids after enzymolysis, it is easier to be digested, absorbed...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/29A23L33/00
CPCA23L33/00A23V2002/00A23V2300/10
Inventor 戴路
Owner HARBIN MO MEDICAL BIOLOGICAL TECH CO LTD
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