Energy-saving preparation technology of high-quality glucose powder

A technology of glucose powder and preparation process, which is applied in the direction of sustainable manufacturing/processing, chemical industry, climate sustainability, etc. It can solve the problems of difficult separation of crystals and mother liquor, high energy consumption of the system, and time-consuming operation, so as to avoid losses and The production of toxic substances, the effect of sufficient separation, and the effect of reducing the content of miscellaneous sugars

Active Publication Date: 2015-05-06
SHANDONG LONGLIVE BIO TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the crystallization of glucose not only requires a large investment in equipment, but also takes up a lot of land, and the operation is very time-consuming. Generally, the cooling crystallization needs to be maintained for about 60 hours.
After glucose crystallization, it is very difficult to separate the crystals from the mother liquor. In industrial production, a centrifuge with high separation factor is used to filter the mother liquor and impurities, which further restricts the production efficiency of the product. In addition, the wet sugar obtained is also need drying
Therefore, the existing crystallization process line of glucose is long, resulting in high cost and low production efficiency.
[0004] Patent CN1928121A "A method for extracting high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024]Get the starch, add process water to adjust the size, control the Baume degree of the starch milk after the size adjustment to be 18, adjust the pH value of the starch milk to 4.8, add liquefying enzyme (i.e. α-amylase) to the starch milk to liquefy, The amount of liquefaction enzyme added is 0.40kg / t starch dry basis. The starch milk is sprayed and liquefied by the liquefaction injector. The injection temperature is 120°C. The feed liquid enters the high temperature maintenance tank for 3 minutes to kill the enzyme. The pH value of the liquefied liquid is controlled at 5.0. The DE value is 14%. After heat exchange, the pH of the liquefied liquid was adjusted to 4.0, and 0.35 kg / t of dry-based saccharification enzyme was added for saccharification, which was kept for 48 hours with intermittent stirring during the process. The DE value was 98.2%, and the glucose content was 96.1%. The above feed liquid is subjected to plate and frame filtration, and the filtrate is subjec...

Embodiment 2

[0026] Get the starch, add process water to adjust the size, control the Baume degree of the starch milk after the size adjustment to be 15, adjust the pH value of the starch milk to 5.0, add liquefying enzyme (i.e. α-amylase) to the starch milk to liquefy, The amount of liquefying enzyme added is 0.35kg / t starch dry basis. The starch milk is sprayed and liquefied through the liquefaction injector. The injection temperature is 105°C. The feed liquid enters the high temperature maintenance tank and keeps for 3 minutes to kill the enzyme. The pH value of the liquefied liquid is controlled at 5.5. The DE value is 19%. After heat exchange, the pH of the liquefied liquid was adjusted to 4.5, and 0.40 kg / t of dry-based carbohydrase was added for saccharification. The heat preservation was carried out for 48 hours, with intermittent stirring during the process. The DE value was 98.1%, and the glucose content was 96.0%. The above-mentioned feed liquid is subjected to plate and frame f...

Embodiment 3

[0028] Get starch, add process water to carry out pulping, control the Baume degree of starch milk after pulping to be 20, adjust the pH value of starch milk to 6.0, add liquefaction enzyme (i.e. α-amylase) to starch milk, carry out liquefaction, The amount of liquefaction enzyme added is 0.30kg / t starch dry basis. The starch milk is sprayed and liquefied by the liquefaction injector. The injection temperature is 135°C. The feed liquid enters the high temperature maintenance tank for 3 minutes to kill the enzyme. The pH value of the liquefied liquid is controlled at 6.0. The DE value is 17%. After heat exchange, the pH of the liquefied liquid was adjusted to 5.0, and 0.45 kg / t of dry-based carbohydrase was added for saccharification. The heat preservation was carried out for 48 hours, with intermittent stirring during the process. The DE value was 98.2%, and the glucose content was 96.1%. The above feed liquid is subjected to plate and frame filtration, and the filtrate is sub...

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PUM

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Abstract

The invention discloses an energy-saving preparation technology of high-quality glucose powder. The technology comprises the following steps: by using starch as a raw material, mixing syrup, liquefying, saccharifying, decoloring and removing impurities by an ultrafiltration membrane, removing salt by ion exchange, purifying by a simulated moving bed, collecting the cut fraction with glucose content of at least 99.5%, and then, performing membrane concentration, vacuum belt drying, cooling and grinding to obtain the finished product of the high-quality glucose powder. According to the preparation technology disclosed by the invention, preparation flows of glucose are shortened, a procedure of evaporation and concentration is replaced by membrane concentration, the steam consumption is reduced, the production cost is lowered, meanwhile, the glucose decomposition loss and production of harmful by-products caused by high temperature concentration of liquid glucose are reduced, and the product quality is improved; the glucose is purified by means of the simulated moving bed technology, so that the content of impure glucose in products is decreased, and the glucose purity is up to more than 99.5%; the glucose syrup is dried by means of vacuum belt drying, and is further ground so as to form the crystalline glucose powder, so that the production efficiency is improved.

Description

technical field [0001] The invention relates to an energy-saving preparation process of high-quality glucose powder, belonging to the technical field of glucose production. Background technique [0002] Glucose, a polyhydroxy aldehyde, is the most widely distributed and important monosaccharide in the world. Pure glucose is a colorless or white crystal, not as sweet as sucrose, and easily soluble in water. Glucose plays a very important role in the field of biology. The metabolic intermediates of living cells will produce glucose, and organisms mainly obtain energy through the metabolism of glucose. In addition, glucose is widely used in food industry, biochemical industry, papermaking, textile and pharmaceutical fields. [0003] At present, the industrialized production of glucose uses starch as a raw material and is prepared by a double-enzyme method. The starch undergoes processes such as liquefaction, saccharification, activated carbon decolorization, ion exchange, vac...

Claims

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Application Information

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IPC IPC(8): C12P19/14C12P19/02
CPCY02P20/10
Inventor 刘宪夫王吉垒葛洪刘伟覃树林肖林
Owner SHANDONG LONGLIVE BIO TECH CO LTD
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