Water-based polishing oil with antibacterial function
A water-based varnish, functional technology, used in biocide-containing paints, antifouling/underwater coatings, coatings, etc., can solve the problems of general dispersion and effect, fast drying speed, low viscosity, etc., to achieve modified Better effect, improved hydrophilicity, uniform distribution effect
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Embodiment 1
[0031] (1) Preparation of silane coupling agent modified inorganic nanoparticles
[0032] Mix nano-titanium dioxide, ethanol, deionized water and silane coupling agent with a weight ratio of 1:40:10:2, and then react in a water bath at 60°C for 12 hours under reflux, then cool down to room temperature, and the product is centrifuged and washed to obtain Silane coupling agent modified inorganic nanoparticles. The particle size of the nano titanium dioxide is 10nm.
[0033] (2) Preparation of nano-titanium dioxide modified water-based acrylic resin solution
[0034] Put 45 parts of deionized water and 2 parts of emulsifier into the reactor and heat to 80°C, then add 10 parts of methyl methacrylate, 10 parts of ethyl methacrylate, 10 parts of styrene, and 20 parts of the product obtained in step (1) The silane coupling agent modified inorganic nanoparticles, 4 parts of polyethylene glycol and 0.4 part of water-soluble initiator are put into the reactor and stirred evenly, after...
Embodiment 2
[0048] (1) Preparation of silane coupling agent modified inorganic nanoparticles
[0049] Mix nano-titanium dioxide, ethanol, deionized water and silane coupling agent with a weight ratio of 1:30:5:1, and then reflux in a water bath at 60°C for 8 hours, then cool down to room temperature, and the product is centrifuged and washed to obtain Silane coupling agent modified inorganic nanoparticles. The particle size of the nano titanium dioxide is 20nm.
[0050] (2) Preparation of nano-titanium dioxide modified water-based acrylic resin solution
[0051] Put 30 parts of deionized water and 1 part of emulsifier into the reactor and heat to 80°C, then modify 10 parts of ethyl methacrylate, 10 parts of methyl acrylate, and 15 parts of silane coupling agent obtained in step (1) Inorganic nanoparticles, 3 parts of polyethylene glycol and 0.25 parts of water-soluble initiator are put into the reactor and stirred evenly. After 0.5 hours of heat preservation, 0.25 parts of water-soluble...
Embodiment 3
[0065] (1) Preparation of silane coupling agent modified inorganic nanoparticles
[0066] Mix nano-titanium dioxide, ethanol, deionized water and silane coupling agent with a weight ratio of 1:50:15:3, and then react in a water bath at 60°C for 16 hours under reflux, then cool down to room temperature, and the product is centrifuged and washed to obtain Silane coupling agent modified inorganic nanoparticles. The particle size of the nano titanium dioxide is 15nm.
[0067] (2) Preparation of nano-titanium dioxide modified water-based acrylic resin solution
[0068] Put 60 parts of deionized water and 3 parts of emulsifier into the reactor and heat to 80°C, then add 20 parts of hydroxyethyl methacrylate, 10 parts of hydroxyethyl methacrylate, 10 parts of styrene, 25 parts of step (1 ) The obtained silane coupling agent modified inorganic nanoparticles, 5 parts of polyethylene glycol and 0.5 part of water-soluble initiator are put into the reactor and stirred evenly, after 1 ho...
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