Composite aerosol fire extinguishing material with bioremediation function and preparation method thereof
A fire extinguishing material and bioremediation technology, applied in fire prevention equipment, etc., can solve the problems of short fire extinguishing distance, high cost, hazards to people and the surrounding environment, etc., and achieve the goal of eliminating toxic substance residues, good anti-reburning performance, and promoting ecological restoration Effect
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Embodiment l
[0010] Inoculate Bacillus subtilis in 5ml LB medium, and carry out shaking culture at 35°C for 12 hours, re-inoculate 1ml of the culture into 100ml spore-forming medium, then shake again at 35°C for 60 hours, collect the fermentation broth, The fermentation broth was centrifuged at 6000r / m for 10 min to obtain the bacteria, and the corresponding bacterial dormant spore solid particles A were prepared by vacuum freeze-drying 。
[0011] In terms of weight percentage, formula 1 using composite aerosol fire extinguishing agent is: potassium nitrate 26%, strontium nitrate 20%, ammonium nitrate 5%, potassium carbonate 4%, magnesium powder 7%, trehalose 1%, lactose 1% , sucrose 1%, guanidine sulfamate 1%, nitroguanidine 0.5%, urotropine 2%, dicyandiamide 0.5%, ammonium hydrogen phosphate 2%, ammonium oxalate 2.5%, sodium stearate 0.5% and poly 3% vinyl alcohol, 3% bacterial dormant spore granules A, 5% superfine ammonium polyphosphate powder and 2% graphite powder, 8% phenolic resin...
Embodiment 2
[0013] Inoculate Bacillus licheniformis in 5ml LB medium, and carry out shaking culture at 35°C for 12 hours, re-inoculate 1ml of the culture into 100ml spore-forming medium, then shake again at 35°C for 72 hours, collect the fermentation broth, The fermentation broth was centrifuged at 6000r / m for 10 min to obtain the bacteria, and the corresponding bacterial dormant spore solid particles B were prepared by vacuum freeze-drying 。
[0014] In terms of weight percentage, formula 2 using composite aerosol fire extinguishing agent is: 40% potassium nitrate, 15% strontium nitrate, 5% ammonium nitrate, 8% magnesium powder, 1% trehalose, 1% lactose, guanidine sulfamate 1%, urotropine 2%, ammonium hydrogen phosphate 2%, ammonium oxalate 5% and polyvinyl alcohol 5%, bacterial dormant spore granules B 2%, superfine ammonium polyphosphate powder 6%, phenolic resin 7%, will All the above solid components were thoroughly ground and mixed, and then weighed 1.4 grams of medicament respecti...
Embodiment 3
[0016]Degradability test of bioremediation agent to oil stains: use the residual powder that the aerosol fire extinguishing agent containing bioremediation agent that this embodiment 2 prepares burns to finish, add according to the amount of 10% of oil weight to the 1000% gasoline that is mixed with 1% gasoline and diesel oil Place in a sealed Erlenmeyer flask in a milliliter of water, and incubate on a shaker at 35°C for 12-24 hours with a rotation speed of 150-250rpm. Add the same weight of distilled water as the blank control. At the end of the cultivation, petroleum ether was added to the culture medium, and the oil-in-water emulsion was broken by centrifugation. The organic phase was filtered and dehydrated with granular anhydrous sodium sulfate and placed in a pre-constant weight beaker. The residual oil content in the culture medium was determined by gravimetric method and gas chromatography. Use the following formula to calculate the biodegradation rate (A) of various...
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