Asphalt resin composite spherical activated carbon with developed apertures and low energy consumption and preparation method thereof

A technology of spherical activated carbon and asphalt resin, which is applied in the field of materials, can solve the problems of high ash content of coal-based activated carbon, limit application and development, and low mechanical strength, achieve high hardness, reduce reaction time and energy consumption, and improve mechanical strength. Effect

Inactive Publication Date: 2015-10-21
ANHUI CHENGFANG NEW MATERIAL TECH
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Problems solved by technology

Among them, coal-based spherical activated carbon has the advantages of cheap raw materials and wide sources, but coal-based ac

Method used

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Embodiment Construction

[0016] specific implementation plan

[0017] The present invention will be described in detail below through specific examples.

[0018] A kind of asphalt resin composite spherical activated carbon with developed pore size and low energy consumption, prepared from the following raw materials in parts by weight (kg): octadecyl acrylate 46, vinyl caproate 39, benzoyl peroxide 2, N, N'-methylenebisacrylamide 1, butanediol 18, ethyl acetate 10, sodium dodecylbenzenesulfonate 1, distilled water, acetone, sulfonated asphalt powder 25, attapulgite 3, nanometer 2 Silicon oxide 2, silane coupling agent kh560 0.8, 15% hydrochloric acid 5, 12% sodium hydroxide solution 5;

[0019] A kind of asphalt resin composite spherical activated carbon with well-developed pore size and low energy consumption described in the present invention is made by the following specific steps:

[0020] (1) Add sodium dodecylbenzenesulfonate to 200 times the amount of distilled water, stir at a speed of 600 r...

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Abstract

The invention discloses asphalt resin composite spherical activated carbon with developed apertures and low energy consumption. The asphalt resin composite spherical activated carbon with the developed apertures and the low energy consumption is characterized by being prepared from the following raw materials including, by weight, 46-50 parts of octadecyl acrylic ester, 39-44 parts of ethylhexanoate, 2-3 parts of benzoyl peroxide, 1-2 parts of N,N'-methylene bisacrylamide, 18-20 parts of butanediol, 10-13 parts of ethyl acetate, 1-2 parts of sodium dodecyl benzene sulfonate, appropriate amount of distilled water, appropriate amount of acetone, 25-28 parts of sulfonated gilsonite powder, 3-4 parts of attapulgite, 2-3 parts of nano-silicon dioxide, 0.8-1 part of a silane coupling agent kh560, 5-6 parts of hydrochloric acid with concentration of 15% and 5-6 parts of a sodium hydroxide solution with concentration of 12%. Through the addition of modified nano-titanium dioxide and the attapulgite, the amount of apertures and the sizes of the apertures of products are increased, reaction time and reaction energy consumption are greatly reduced through process innovation, the industrial production is easy to achieve, the hardness is large, and the recycling can be achieved.

Description

technical field [0001] The invention relates to the field of materials, in particular to pitch resin composite spherical activated carbon with developed pore size and low energy consumption and a preparation method thereof. Background technique [0002] Spherical activated carbon has been widely used in related fields such as medicine, environmental protection and catalyst carrier because of its good sphericity, high packing density, less particle shedding and fast adsorption and desorption speed. Spherical activated carbon is mainly divided into three categories according to different raw materials: coal-based spherical activated carbon, polymer resin-based spherical activated carbon and pitch-based spherical activated carbon. Among them, coal-based spherical activated carbon has the advantages of cheap raw materials and wide sources, but coal-based activated carbon has high ash content, many impurities, and low mechanical strength, which limits its application and developm...

Claims

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Application Information

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IPC IPC(8): C01B31/08
Inventor 沈向洋吴克余志敏蒋涌吴杰吴育兵樊云
Owner ANHUI CHENGFANG NEW MATERIAL TECH
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