Laser-marked PBT material with epoxy resin cohesiveness and preparation technology of laser-marked PBT material
A technology of laser marking and epoxy resin, which is applied in the field of polymer materials, can solve the problems of reduced packaging efficiency, difficulty in controlling the curing process of epoxy resin viscosity changes, etc., and achieve the effect of improving adhesion, good marking effect, and small dosage
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[0027] Weighing: PBT 70 kg, cardanolamine 18 kg, polyvinyl alcohol microspheres 18 kg, sodium dodecyl sulfonate 6 kg, gelatin 6 kg, glass fiber 8 kg, silicone powder 2 kg, laser marking powder 4 kg, antioxidant 245 2 kg;
[0028] The laser marking powder is formed by mixing graphene, bismuth oxide and pearlescent powder, and its weight ratio is 2:1:1.
[0029] Specific steps are as follows:
[0030] (1), preparation of microcapsule curing agent:
[0031] ①. Under stirring conditions, add 0.5wt% gelatin aqueous solution and 0.5wt% sodium dodecylsulfonate aqueous solution, and disperse for 40 minutes under mechanical stirring at 800 rpm to obtain an aqueous phase;
[0032] 2. In the dichloromethane solvent, add cardanolamine and polyvinyl alcohol microspheres, and disperse evenly in an ultrasonic instrument to obtain an oil phase, and gradually add the water phase prepared in step 1 into the oil phase;
[0033] ③. Stir and emulsify the mixed solution for 60 minutes, raise the...
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