Preparation method of peanut shell based foam carbon
A technology of peanut shells and foamed carbon, applied in the field of foamed carbon, can solve the problems of low preparation cost, brittleness and brittleness, limited raw material resources, etc., and achieve the effects of large specific surface area, strong adsorption capacity and low preparation cost
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example 1
[0022] First, weigh 1 kg of peanut shells and put them into an airflow mill to crush them, pass through a 100-mesh standard sieve to obtain peanut shell powder, put them in an oven and dry them at 105 °C for 6 hours, weigh 200 g of dried peanut shell powder, and put them into a mixer and reflux Add 1L bamboo tar and 200mL mixed acid solution to the three-necked flask of the device, move the flask into an oil bath at 130°C, start the stirrer to keep warm and reflux for 1 hour; after the above reaction is completed, cool the reaction solution to room temperature, Add 800mL of absolute ethanol, stir with a stirring bar for 20min, filter to remove the filter residue, obtain the filtrate, transfer the filtrate to a rotary evaporator, and remove the absolute ethanol by rotary evaporation at 45°C to obtain liquefied peanut shells; measure 700mL of mass concentration to be 30 % formaldehyde solution and 200mL deionized water were added to the liquefied peanut shells obtained above, sti...
example 2
[0026] First, weigh 1.5kg of peanut shells and put them into an airflow mill to crush them, pass through a 100-mesh standard sieve to obtain peanut shell powder, put them in an oven and dry them at 108°C for 7 hours, weigh 250g of dried peanut shell powder and put them into a mixer and Add 1.5L bamboo tar and 250mL mixed acid solution to the three-necked flask of the reflux device, move the flask into an oil bath at 135°C, start the stirrer to keep warm and reflux for 1.5h; after the above reaction is completed, cool the reaction solution to room temperature , add 850mL of absolute ethanol to it, stir with a stirring bar for 25min, filter to remove the filter residue, obtain the filtrate, transfer the filtrate to a rotary evaporator, and remove the absolute ethanol by rotary evaporation at 50°C to obtain liquefied peanut shells; measure 750mL of mass Add 30% formaldehyde solution and 250mL deionized water to the liquefied peanut shells obtained above, stir with a mixer, add 1...
example 3
[0030] First, weigh 2kg of peanut shells and put them into an airflow mill to crush them, pass through a 100-mesh standard sieve to obtain peanut shell powder, put them in an oven and dry them at 110°C for 8 hours, weigh 300g of dried peanut shell powder and put them into a mixer and reflux Add 2L bamboo tar and 300mL mixed acid solution to the three-necked flask of the device, move the flask into an oil bath at 140°C, start the stirrer to keep warm and reflux for 2 hours; after the above reaction is completed, cool the reaction solution to room temperature, Add 900mL of absolute ethanol, stir with a stirring bar for 30min, filter to remove the filter residue, obtain the filtrate, transfer the filtrate to a rotary evaporator, and remove the absolute ethanol by rotary evaporation at 55°C to obtain liquefied peanut shells; measure 800mL with a mass concentration of 30 % formaldehyde solution and 300mL deionized water were added to the liquefied peanut shells obtained above, stirr...
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