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A kind of polyester resin solid lubricating block and preparation method thereof

A technology of polyester resin and solid lubrication, applied in lubricating compositions, petroleum industry, etc., can solve the problems of accelerated release rate of solid lubricating block, unstable relative size of lubricating block, influence of high temperature resistance, etc., and achieve excellent self-lubricating performance , Conducive to environmental protection, good hardness effect

Active Publication Date: 2020-05-01
ANHUI UNIVERSITY OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage is that the high temperature resistance is affected, and the release rate of the solid lubricating block will be accelerated under high temperature conditions
[0008] Patent CN201520403670.8 provides a self-lubricating block structure, which is characterized by the use of rare earth oil-containing nylon polymer materials, which increases self-lubricating properties, and also has excellent self-lubricating effects in the case of oil-free lubrication, which can effectively It solves the problem of solidification of lubricating oil in severe cold climates, the decrease of lubricating performance and damage to the equipment itself, and the problem of damage to the equipment caused by dust particles entering the slide rails for grinding when operating in high temperature and high dust environments in summer
The disadvantage is that the lubricating block is relatively unstable in size and is easily affected by water vapor
The disadvantage of the two is that the solid lubricating block is prepared under high temperature conditions, and the molding process is relatively complicated

Method used

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  • A kind of polyester resin solid lubricating block and preparation method thereof
  • A kind of polyester resin solid lubricating block and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] (1) Take unsaturated polyester resin 10g, reactive diluent hydroxyethyl acrylate 1g, promotor cobalt isooctanoate 1.0g, the weight ratio of talcum powder, graphite and nano-magnetic particle iron tetroxide three is 8:1: 1, 5g of lubricating filler, 6g of emulsified oil, and 1g of methyl silicone oil.

[0036] (2) Mix the weighed unsaturated polyester resin and lubricating filler evenly, then add methyl silicone oil, active diluent and accelerator and stir evenly with a glass rod.

[0037] (3) Weigh again 10 g of modified hollow glass microspheres, then add 3.33 g of curing agent methyl ethyl ketone peroxide, and mix well.

[0038] (4) Mix the unsaturated polyester resin formula mixed in (3) with emulsified oil.

[0039](5) Apply the release agent to the inner surface of the mold with a brush, and pour the mixture of (4) into the mold to cure at room temperature.

Embodiment 2

[0041] (1) Take unsaturated polyester resin 10g, promotor lead naphthenate 2.0g, reactive diluent hydroxyethyl methacrylate 1g, talcum powder, graphite and nano magnetic particle triiron tetroxide weight ratio are 7.5 :1.5:1 lubricating filler 5g, emulsified oil 6g, methyl silicone oil 0.67g.

[0042] (2) Mix the weighed unsaturated polyester resin and lubricating filler evenly, then add methyl silicone oil, active diluent and accelerator and stir evenly with a glass rod.

[0043] (3) Weigh again 10 g of modified hollow glass microspheres, then add 1.5 g of curing agent benzoyl peroxide, and mix well.

[0044] (4) Mix the unsaturated polyester resin formula mixed in (3) with emulsified oil.

[0045] (5) Apply the release agent to the inner surface of the mold with a brush, and pour the mixture of (4) into the mold to cure at room temperature.

Embodiment 3

[0047] (1) Take by weighing unsaturated polyester resin 10g, reactive diluent trimethylolpropane triacrylate 0.67g, promotor cobalt isooctanoate 1.0g, talc powder, graphite and nano magnetic particle ferric oxide three weight ratios 7:2:1 lubricating filler 2.0g, emulsified oil 6g, methyl silicone oil 1g.

[0048] (2) Mix the weighed unsaturated polyester resin and lubricating filler evenly, then add methyl silicone oil, active diluent and accelerator and stir evenly with a glass rod.

[0049] (3) Weigh again 10 g of modified hollow glass microspheres, then add 1.34 g of curing agent cumene hydroperoxide, and mix well.

[0050] (4) Mix the unsaturated polyester resin formula mixed in (3) with emulsified oil.

[0051] (5) Apply the release agent to the inner surface of the mold with a brush, and pour the mixture of (4) into the mold to cure at room temperature.

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Abstract

The invention discloses a polyester resin solid lubrication block and a preparation method thereof, and belongs to the field of solid lubrication materials. The polyester resin solid lubrication block is prepared from the following components in parts by weight: 30-45 parts of unsaturated polyester resin, 25-35 parts of modified hollow glass beads, 8-20 parts of emulsified oil, 5-15 parts of lubrication-assisting packing, 3-7 parts of an accelerant, 4-10 parts of a curing agent, 2-5 parts of methylsilicone oil and 2-4 parts of a reactive diluent. The prepared lubrication block has good hardness and an extremely low friction coefficient, and can be widely applied to a heavy-load sliding or rolling friction pair; distillated residue oil obtained from stearic acid is prepared by employing palm oil hydrolysis, comprehensive utilization of resources is achieved, lubricating grease does not need to be added, the polyester resin solid lubrication block has excellent self-lubricating property, and is beneficial to environment protection and iron and steel resource conservation, and a high polymer material is light and beneficial to reduction of mechanical loads.

Description

technical field [0001] The invention belongs to the field of solid lubricating materials, and in particular relates to a solid lubricating block and a preparation method thereof. Background technique [0002] In recent years, with the development of science and technology, higher and higher requirements have been put forward for the performance of various equipment and parts. Friction and wear is a common natural phenomenon. Statistics from the World Society of Tribology show that more than 1 / 3 of the world's primary energy is lost by friction, and the annual loss caused by wear and tear accounts for about 1% of the gross national product. In order to prolong the service life, save materials and energy, it is urgent to solve the problems of friction, wear and lubrication protection in many fields. [0003] There are four types of lubricating materials: gas lubricants, fluids (mainly oil), grease (semi-solid) and solid lubricating materials. Liquid and semi-solid lubricatio...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M169/04C10M177/00C10N30/04C10N30/06C10N50/08
CPCC10M169/04C10M177/00C10M2201/041C10M2201/062C10M2201/102C10M2201/14C10M2203/06C10M2207/06C10M2207/126C10M2207/16C10M2207/281C10M2207/283C10M2207/289C10M2207/40C10M2209/102C10M2229/041C10N2030/04C10N2030/06C10N2050/08C10N2020/02
Inventor 田雪梅王圣达姚军乔红斌吴胜华古绪鹏陈国昌
Owner ANHUI UNIVERSITY OF TECHNOLOGY
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