A kind of doped carbon material and preparation method thereof
A carbon material and ball milling technology, which is applied in the preparation of amino compounds, chemical instruments and methods, catalyst activation/preparation, etc., can solve the problems of harsh preparation conditions and expensive raw materials, and achieve simple preparation process, simple preparation and high yield Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0034] This embodiment provides a doped carbon material, which is prepared by the following steps:
[0035] Ball mill the graphite at 750 rpm for 48 hours to obtain ball milled graphite;
[0036] Weigh 2g of ball-milled graphite and immerse it in 80mL of ethanol, add 10g of boric acid, and stir through ultrasonic to obtain a mixture;
[0037] Place the mixture in a heating device at 80°C to remove ethanol to obtain a solid phase mixture;
[0038] Put the solid phase mixture into a horizontal tube furnace, calcinate at 900°C for 2h in a nitrogen atmosphere, and take it out after cooling to room temperature;
[0039] The calcined product was washed with warm water at 60° C.-100° C. and dried in an oven to obtain 1.75 g of doped carbon material with a yield of 88%.
[0040] The above-mentioned doped carbon material of this embodiment is analyzed by XPS, such as figure 1 Shown. figure 1 It can be seen that there is boron in the doped carbon material, and the boron content is 3.92at%.
[0041]...
Embodiment 2
[0047] This embodiment provides a doped carbon material, which is prepared by the following steps:
[0048] Ball mill the graphite at 750 rpm for 48 hours to obtain ball milled graphite;
[0049] Weigh 2g of ball-milled graphite and immerse it in 80mL of ethanol, add 10g of boric acid, and stir through ultrasonic to obtain a mixture;
[0050] Place the mixture in a heating device at 80°C to remove ethanol to obtain a solid phase mixture;
[0051] Put the solid phase mixture into a horizontal tube furnace, calcinate at 1000°C for 2h under a nitrogen atmosphere, and take it out after cooling to room temperature;
[0052] The calcined product was washed with warm water at 60-100° C. and dried in an oven to obtain 1.64 g of doped carbon material with a yield of 82%.
[0053] The above-mentioned doped carbon material of this embodiment is analyzed by XPS, such as Figure 5 Shown. Figure 5 It can be seen that there is boron in the doped carbon material, and the boron content is 9.65 at%.
[...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More