Preparation method of yttrium oxide photoexcited synergistically fine-grained high-alumina bronze indicator coating

A high-aluminum bronze, fine-grain strengthening technology, applied in coating, metal material coating process, melt spraying and other directions, can solve the problems of high cost of production data, difficult to promote, etc., to achieve process stability and repeatability, High-precision component control effect

Active Publication Date: 2019-09-03
LANZHOU UNIVERSITY OF TECHNOLOGY +1
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  • Summary
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  • Description
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  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Wear detection is an important way to evaluate the wear degree of materials. Commonly used wear detection technologies include acoustic emission, photothermal radiation, dynamometer, vibration, ferrography, etc. Since these detection technologies realize wear evaluation through the development of advanced sensors and other equipment, the cost High and requires rich production data, not easy to promote

Method used

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  • Preparation method of yttrium oxide photoexcited synergistically fine-grained high-alumina bronze indicator coating
  • Preparation method of yttrium oxide photoexcited synergistically fine-grained high-alumina bronze indicator coating

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preparation example Construction

[0020] A preparation method of yttrium oxide photoexcited synergistically fine-grained high-alumina bronze indicator coating, comprising the following steps:

[0021] (1) Clean the surface of the 45# steel substrate with ultrasonic waves, use a semi-automatic acid spraying machine to roughen the sprayed welding surface of the substrate after cleaning, the diameter of the nozzle is 0.5mm, the amount of acid sprayed is 20ml / min, and the acid component: 27ml of nitric acid , hydrofluoric acid 62ml, distilled water 270ml.

[0022] (2) Put the treated substrate into a heat treatment furnace to preheat to 260°C-300°C, and the preheating heating rate is 10°C / min;

[0023] (3) Weigh high-alumina bronze powder and yttrium oxide powder according to the mass percentage of 99.4-99.8:0.2-0.6, perform mechanical alloying in a stirring ball mill, the rotor speed is 290 rpm, and the grinding ball is 3mm ZrO 2 Ball, ball milling time 25 hours, ball milling medium is absolute ethanol, material...

Embodiment 1

[0027] (1) Clean the surface of 45# steel substrate with ultrasonic waves, and use a semi-automatic acid spraying machine to roughen the sprayed welding surface of 45# steel substrate after cleaning. The diameter of the nozzle is 0.5mm, and the amount of acid sprayed is 20ml / min. : Nitric acid 27ml, hydrofluoric acid 62ml, distilled water 270ml;

[0028] (2) Put the treated substrate into a heat treatment furnace to preheat to 270°C, and the preheating heating rate is 10°C / min;

[0029] (3) Weigh the high-alumina bronze powder and yttrium oxide powder according to the mass percentage of 99.4:0.6, carry out mechanical alloying in the stirring ball mill, the rotor speed is 290 rpm, and the grinding ball is 3mm ZrO 2 Balls, the ball milling time is 25 hours, the ball milling medium is absolute ethanol, according to the mass ratio, material: ball: absolute ethanol = 1:18:0.2;

[0030] (4) Dry the powder with a high-speed centrifugal spray dryer, the rotational speed of the centri...

Embodiment 2

[0032] (1) Clean the surface of 45# steel substrate with ultrasonic waves, and use a semi-automatic acid spraying machine to roughen the sprayed welding surface of 45# steel substrate after cleaning. The diameter of the nozzle is 0.5mm, and the amount of acid sprayed is 20ml / min. : Nitric acid 27ml, hydrofluoric acid 62ml, distilled water 270ml;

[0033] (2) Put the treated substrate into a heat treatment furnace to preheat to 290°C, and the preheating heating rate is 10°C / min;

[0034] (3) Weigh the high-alumina bronze powder and yttrium oxide powder according to the mass percentage of 99.6:0.4, carry out mechanical alloying in the stirring ball mill, the rotor speed is 290 rpm, and the grinding ball is 3mm ZrO 2 Balls, the ball milling time is 25 hours, the ball milling medium is absolute ethanol, according to the mass ratio, material: ball: absolute ethanol = 1:18:0.2;

[0035] (4) Dry the powder with a high-speed centrifugal spray dryer, the rotational speed of the centri...

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Abstract

The invention discloses a method for preparing a high-alumina bronze indicating coating through optical excitation in collaboration with fine grain strengthening of yttrium oxide. The surface of a 45# steel substrate is cleaned through ultrasonic waves, the spraying welding surface of the cleaned 45# steel substrate is subjected to roughening treatment through an acid spraying technique, and the treated substrate is placed into a heat treatment furnace to be preheated till the temperature is 260-300 DEG C; and high-alumina bronze powder and yttrium oxide powder are weighed according to the mass percent of (99.4-99.8):(0.2-0.6), and are subjected to mechanical alloying in a stirring ball mill, the powder is dried, is subjected to ball milling and is loaded into a welding gun, and the high-alumina bronze indicating coating is prepared on the preheated 45# steel substrate through a plasma spraying welding machine under the conditions that the transfer arc current is 165-175 A, the working voltage is 25.4-26 V, the powder feeding quantity is 17-21 g / min, and the distance of the welding gun and a workpiece is 8-11 mm.

Description

technical field [0001] The invention relates to a self-sensitive luminescent on-line monitoring technology for worn and corroded surfaces, in particular to a method for preparing a high-alumina bronze coating doped with yttrium oxide fluorescent particle function indication. Background technique [0002] Wear detection is an important way to evaluate the wear degree of materials. Commonly used wear detection technologies include acoustic emission, photothermal radiation, dynamometer, vibration, ferrography, etc. Since these detection technologies realize wear evaluation through the development of advanced sensors and other equipment, the cost High and requires rich production data, it is not easy to promote. [0003] Using a luminescent coating to monitor wear and corrosion surfaces on-line will greatly reduce the requirements for sensors and other components and simplify the operation process. That is to say, the luminescent particles are incorporated into the wear-resista...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C4/134C23C4/06C23C4/11
Inventor 李文生董洪峰胡春霞杨效田何玲冯力安国升
Owner LANZHOU UNIVERSITY OF TECHNOLOGY
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