A kind of environment-friendly quenching liquid and preparation method thereof
A kind of quenching liquid, environmental protection technology, applied in the direction of quenching agent, manufacturing tools, heat treatment equipment, etc., can solve the problems of difficult control of the production process, poor anti-rust performance, easy to breed bacteria, etc., to achieve good anti-rust effect and good bactericidal effect. , the effect of improving the working environment
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Embodiment 1
[0031] Add 100kg ISALCHEM145 isomerized alcohol (produced by Sasol, the main component is C14 / 15 isomerized alcohol, containing a small amount of C13 and below, C16 and above isomerized alcohol), 15kg potassium hydroxide solution (concentration 20%) into the polymerization kettle , with ice-salt water circulation cooling at around 0°C, and at the same time pass nitrogen into the polymerization kettle to replace the air in the kettle. When the nitrogen in the kettle maintains positive pressure, feed 100kg ethylene oxide and 100kg propylene oxide Send them into the kettle respectively, while stirring and raising the temperature to 120°C. The pressure in the kettle is kept not more than 0.5MPa. After 12 hours of polymerization, the polymer in the polymerization kettle is discharged, which is the polymerization of isomeric alcohol polyoxyethylene polyoxypropylene ether. things. It can be used as a quenching liquid composition.
[0032] The isomeric alcohol polyoxyethylene polyoxy...
Embodiment 2
[0041] Add 100kg of Synative ALG16 isomeric alcohol (manufactured by BASF, the main component is C16 isomeric alcohol), 15kg of sodium hydroxide solution (10% concentration) into the polymerization kettle, and circulate and cool with ice salt water at about 0°C. Introduce nitrogen into the kettle to replace the air in the kettle. When the nitrogen in the kettle maintains a positive pressure, feed 150kg of ethylene oxide and 50kg of propylene oxide mixture into the kettle with nitrogen feed tank, and stir at the same time to raise the temperature to 100°C. The pressure is kept not greater than 0.5 MPa, and after 12 hours of polymerization, the polymer in the polymerization tank is discharged, which is the isomeric alcohol polyoxyethylene polyoxypropylene ether polymer.
[0042] The isomeric alcohol polyoxyethylene polyoxypropylene ether polymer prepared by the above method has the following physical and chemical indicators after testing:
[0043] project
basic data...
Embodiment 3
[0050] 200kg SAFOL23 isomeric alcohols (production of Sasol company, main component is C12 / C13 isomeric alcohols, containing a small amount of C11 and C14 isomeric alcohols), 22kg potassium hydroxide solution (concentration 15%) are added in the polymerization kettle, with 0 The ice salt water at about ℃ is circulated and cooled, and at the same time, nitrogen is introduced into the polymerization kettle to replace the air in the kettle. When the nitrogen in the kettle maintains a positive pressure, 240kg of ethylene oxide and 160kg of propylene oxide are respectively fed into In the kettle, stir and raise the temperature to 110°C at the same time, and keep the pressure in the kettle not greater than 0.5MPa. After 12 hours of polymerization, the polymer in the polymerization kettle is discharged, which is the isomeric alcohol polyoxyethylene polyoxypropylene ether polymer.
[0051] Add 15kg potassium molybdate, 12kg potassium sorbate, and 120kg star anise extract into 753kg wat...
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