Method for increasing dyeing depth of para-aramid fibers and fabrics
A technology for dyeing para-aramid fibers and fabrics. It is applied in the direction of dyeing, textiles and papermaking. It can solve the problems of deep color, insufficient color fastness, high dyeing temperature, and easy occurrence of color flowers, so as to improve the dyeing effect, Expand the scope of application and improve the effect of dyeing depth
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Embodiment 1
[0026] Example 1: Plasma treatment or ultrasonic treatment of para-aramid short fibers using argon and oxygen mixed gas (or nitrogen, air is the same), take 5 g of para-aramid short fibers obtained by mechanical processing, and add Pretreatment agent 8g / L compounded by sodium hydroxide (concentration 5g / L) and scouring agent (concentration 4g / L), soft water 100mL (bath ratio 1:20), heated at 80°C for 20min, and then washed with water Removes surface oils. The degreased fiber is treated with high frequency by ultrasonic processor. Take by weighing Disperse Red A2 dyestuff 0.15g (dyeing concentration 3%) in beaker, add 75mL soft water (bath ratio 1:30), add by Cindy DNK (concentration 20g / L), fatty alcohol polyoxyethylene ether sodium sulfate (concentration 5g / L), sodium chloride (concentration 10g / L), 2.5g of dyeing auxiliaries, stirred and heated to about 60°C to disperse and mix the dyes and dyeing auxiliaries evenly, then adjust the pH with acetic acid / sodium acetate buffer...
Embodiment 2
[0027] Embodiment 2: get para-aramid filament 5g, add the pretreatment agent 8g / L compounded by sodium carbonate (concentration 8g / L) and scouring agent (concentration 5g / L) in Erlenmeyer flask, soft water 50mL (bath Ratio 1:10), heated at 90°C for 15 minutes, then washed with water to remove surface oil. And carry out high-speed agitation and cleaning in a washer with stirring for 10 minutes. Take by weighing Disperse Red A9 dyestuff 0.125g (dyeing concentration 2.5%) in beaker, add 80mL (bath ratio 1:16) (soft water, add by Cindy DNK (concentration 40g / L), fatty alcohol polyoxyethylene ether sodium sulfate ( Concentration 8g / L), sodium chloride (concentration 20g / L) compound dyeing auxiliaries 30g / L, stir and heat to about 60°C to disperse and mix the dyes and dyeing auxiliaries evenly, then use acetic acid / sodium acetate buffer solution Adjust the pH value to 4, and pour the prepared dye solution into the dyeing cup. Take the treated para-aramid fiber and put it into the d...
Embodiment 3
[0028]Embodiment 3: Get 5g of para-aramid filaments, and add preform compounded by sodium hydroxide (concentration 3g / L), sodium carbonate (concentration 3g / L) and scouring agent (concentration 5g / L) in the Erlenmeyer flask Treating agent 6g / L, soft water 70mL (bath ratio 1:14), heat at 90°C for 15min, then wash with water to remove surface oil. And wash it in a high-frequency ultrasonic cleaner for 20 minutes. Weigh 0.15 g of disperse blue B1 dye (dyeing concentration 3%) in a beaker, add 90 mL soft water (bath ratio 1:16), add HPS-301 (concentration 30 g / L), fatty alcohol polyoxyethylene ether sodium phosphate ( Concentration 8g / L), sodium sulfate (concentration 10g / L) compound dyeing auxiliaries 60g / L, stir and heat to about 60°C to disperse and mix the dyes and dyeing auxiliaries evenly, then adjust with acetic acid-sodium acetate buffer solution When the pH value is 3, pour the prepared dye solution into the dye cup. Take the treated fiber and put it into the dyeing cup...
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