A kind of preparation method of high-gloss and weather-resistant water-based varnish protective varnish for wallpaper
A technology for protecting varnish and weather resistance, used in papermaking, paper coatings, textiles and papermaking, etc., can solve the problems of waterproof and moisture-proof, poor weather resistance, wall warping and falling off, reduced service life and aesthetics, etc., to achieve good gloss. , strong adhesion, excellent anti-permeability effect
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Embodiment 1
[0025] A preparation method for high-gloss and weather-resistant water-based varnish protective varnish for wallpaper, comprising the following steps:
[0026] Step 1. Weigh fullerene and dissolve it completely in toluene to form solution A; weigh silver nitrate and dissolve it completely in acetonitrile to form solution B; wherein the concentration ratio of solution A to solution B is 1 : 4~5; According to the ratio of 1mL: 1mL: 0.5g, take solution A, solution B and citric acid for mixing in turn, put the mixed solution in an autoclave, react at 130°C for 10h, cool, pump filtered, and the filtrate was washed with absolute ethanol and dried to obtain modified fullerene; mixed and stirred with propylene glycol methyl ether and modified fullerene, and then heated in an argon atmosphere at 95°C for 2 hours , add acrylic acid monomer, and react at 100°C for 6h, cool down, and remove propylene glycol methyl ether under reduced pressure, and the final product is filtered, dried, and...
Embodiment 2
[0035] A preparation method for high-gloss and weather-resistant water-based varnish protective varnish for wallpaper, comprising the following steps:
[0036] Step 1. Weigh fullerene and dissolve it completely in toluene to form solution A; weigh silver nitrate and dissolve it completely in acetonitrile to form solution B; wherein the concentration ratio of solution A to solution B is 1 : 4~5; According to the ratio of 1mL: 1mL: 0.1g, take solution A, solution B and citric acid for mixing in turn, put the mixed solution in an autoclave, react at 130°C for 7h, cool, pump filtered, and the filtrate was washed with absolute ethanol and dried to obtain modified fullerene; mixed and stirred with propylene glycol methyl ether and modified fullerene, and then heated in an argon atmosphere at 80°C for 2 hours , add acrylic acid monomer, and react at 100°C for 5 hours, cool, and remove propylene glycol methyl ether under reduced pressure, and the final product is filtered, dried, and ...
Embodiment 3
[0041] A preparation method for high-gloss and weather-resistant water-based varnish protective varnish for wallpaper, comprising the following steps:
[0042] Step 1. Weigh fullerene and dissolve it completely in toluene to form solution A; weigh silver nitrate and dissolve it completely in acetonitrile to form solution B; wherein the concentration ratio of solution A to solution B is 1 : 4~5; According to the ratio of 1mL: 1mL: 0.3g, take solution A, solution B and citric acid for mixing in turn, put the mixed solution in an autoclave, react at 130°C for 8h, cool, pump filtered, and the filtrate was washed with absolute ethanol and dried to obtain modified fullerene; mixed and stirred with propylene glycol methyl ether and modified fullerene, and then heated in an argon atmosphere at 100°C for 1 h , add acrylic acid monomer, and react at 100°C for 6h, cool down, and remove propylene glycol methyl ether under reduced pressure, and the final product is filtered, dried, and gro...
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