Butyl rubber reactive bonding layer used for pre-paving reactive-bonding waterproofing coiled material, preparation method thereof, and the pre-paving reactive-bonding waterproofing coiled material

A waterproof membrane and reactive adhesive technology, which is applied in the direction of adhesives, layered products, polymer adhesive additives, etc., can solve the problems of inconvenient identification of leaking points, easy flow, and restrictions on the application fields of pre-laid reactive adhesive membrane construction, etc. question

Active Publication Date: 2018-01-19
BEIJING ORIENTAL YUHONG WATERPROOF TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At this stage, the polymer waterproof membrane adhesive layer is commonly used in underground buildings, most of which are hot-melt pressure-sensitive adhesive systems. Anti-adhesive layer or isolation layer, in order to not stick to the feet, easy to construct and form a bond with the cured concrete; the peel strength between the adhesive layer and the post-cast concrete is low; there are also a small part of the reactive adhesive layer that is black butyl Adhesive layer, it is not easy to identify the leakage point, which limits the construction application field of pre-laid reactive adhesive membrane

Method used

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  • Butyl rubber reactive bonding layer used for pre-paving reactive-bonding waterproofing coiled material, preparation method thereof, and the pre-paving reactive-bonding waterproofing coiled material
  • Butyl rubber reactive bonding layer used for pre-paving reactive-bonding waterproofing coiled material, preparation method thereof, and the pre-paving reactive-bonding waterproofing coiled material
  • Butyl rubber reactive bonding layer used for pre-paving reactive-bonding waterproofing coiled material, preparation method thereof, and the pre-paving reactive-bonding waterproofing coiled material

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preparation example Construction

[0140] According to a second aspect of the present invention, there is provided a method for preparing the above-mentioned butyl glue reactive adhesive layer for pre-laying reactive adhesive waterproof membrane, comprising the following steps:

[0141] (a) mix raw rubber with 50-60% of the linear tackifying resin containing terminal hydroxyl structure, the active filler of the formula weight and optional terpene resin, petroleum resin, nano-calcium carbonate, processing aid according to the formula weight additives, inorganic dyes, anti-aging agents and anti-ultraviolet absorbers for banburying;

[0142] (b) After cooling down, continue banburying and molding with the linear tackifying resin containing terminal hydroxyl structure of the remaining formula weight and optional crosslinking agent and reactive auxiliary agent to obtain a butyl rubber reaction adhesive layer.

[0143] The types and sources of the raw materials for the preparation of the butyl rubber reaction adhesiv...

Embodiment 1

[0165] A butyl rubber reaction adhesive layer, consisting of the following raw materials in parts by weight: 100 parts of butyl rubber, 9.5 parts of polyamide-modified novolac resin, 1 part of terpene resin, 5 parts of petroleum resin, and 50 parts of nano-calcium carbonate 12.5 parts of active filler, 10 parts of dioctyl phthalate, 5 parts of titanium dioxide, 1 part of anti-aging agent RD, 1 part of anti-ultraviolet absorber UV-P, 0.5 part of sulfur and 1 part of sodium carboxylate.

[0166] Processing technology: Put butyl rubber in an internal mixer according to the formula weight, process it for 5 minutes at a temperature of 105°C and a speed of 60r / min, and then alternately add terpene resin, petroleum resin, nano-calcium carbonate, Active filler, dioctyl phthalate, titanium dioxide, anti-aging agent RD and anti-ultraviolet absorber UV-P and the polyamide-modified novolac resin of formula weight 60%, banburying 10min, to mixing; The temperature drops to 70°C, add polyami...

Embodiment 2

[0168] A butyl rubber reaction adhesive layer, consisting of the following raw materials in parts by weight: 60 parts of butyl rubber, 40 parts of brominated butyl rubber, 4.5 parts of polyamide-modified novolac resin, epoxy-modified novolak 6.5 parts of phenolic resin, 3 parts of terpene resin, 6 parts of petroleum resin, 80 parts of nano-calcium carbonate, 16 parts of active filler, 20 parts of paraffin oil, 5 parts of iron oxide blue, 1 part of antioxidant 4010NA, anti-ultraviolet absorber UVP- 327 1 part, p-benzoquinone dioxime 0.5 part and sodium citrate 1 part.

[0169] Processing technology: Put butyl rubber and bromobutyl rubber in an internal mixer according to the formula weight, process at a temperature of 105°C and a speed of 60r / min for 8 minutes, then add terpene resin and petroleum in three times alternately Resin, nano-calcium carbonate, active filler, paraffin oil, iron oxide blue, antioxidant 4010NA and anti-ultraviolet absorber UVP-327 and the polyamide-modi...

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Abstract

The invention discloses a butyl rubber reactive bonding layer used for a pre-paving reactive-bonding waterproofing coiled material, a preparation method thereof, and the pre-paving reactive-bonding waterproofing coiled material, and relates to the technical field of high-molecular pre-pavement materials. The butyl rubber reactive bonding layer is mainly produced from: 100 parts of raw rubber, 9.5-15.5 parts of a linear tackifying resin containing terminal hydroxyl group structure, and 12.5-19.5 parts of active filler comprising active silicon dioxide and aluminum oxide. The reactive bonding layer solves the defects that a bonding layer of a waterproofing coiled material in the prior art is liable to flow, deform and wrinkle when being heated, is brittle at low temperature, is free of sticking feet only if a single anti-sticking layer or insulation layer exists, and is poor in stripping strength with post-poured concreted. The butyl rubber reactive bonding layer can form permanent chemical bonds with concrete, so that a real skin-type water-proofing structure is formed between the pre-paved high-molecular waterproofing coiled material and the concrete, and the bonding layer is freeof sticking feet and allows people to walk thereon without coverage by sand and coating layers. In addition, the reactive bonding layer has good low temperature resistance and thermal stability.

Description

technical field [0001] The invention relates to the technical field of polymer pre-laying materials, in particular to a butyl adhesive reactive adhesive layer used for pre-laying reactive adhesive waterproof membranes, a preparation method thereof, and pre-layed reactive adhesive waterproof membranes. Background technique [0002] Building waterproofing is a measure taken to resist external rainwater and groundwater leakage in projects such as walls, roofs, tunnels, highways, underground garages, and residential buildings. It is the first barrier for the entire project and buildings. It plays a vital role. [0003] The polymer pre-paved reactive adhesive waterproofing membrane is suitable for waterproofing basements, reservoirs, roofs, interior and exterior walls of various civil and industrial buildings. In addition, it can also be used for anti-seepage and anti-leakage of various sewage treatment plants, swimming pools, etc., and waterproof and anti-seepage of various und...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J123/22C09J123/28C09J11/04C09J11/08B32B7/12
CPCB32B7/12C09J11/04C09J11/08C09J123/22C09J123/28C08L61/14C08K3/36C08K3/22C08L23/28C09J2301/408B32B7/10C08K2003/2227C09J11/06
Inventor 熊玉钦杨宁徐恩顺谭宁刘阳
Owner BEIJING ORIENTAL YUHONG WATERPROOF TECH CO LTD
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