Graphene composite PP fibers and preparation method thereof
A graphene composite, graphene technology, applied in the direction of melt spinning, single-component polyolefin rayon, etc., can solve the problems of polymer performance, poor toughness at fiber agglomeration, unable to improve fiber performance, etc. Good electrostatic performance
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[0037] A preparation method of graphene composite PP fiber, comprising the following steps: step 1, heating and melting half of the PP (polypropylene) composite masterbatch to obtain a composite masterbatch melt; step 2, dissolving PP in a solvent, adding anion Stir and disperse evenly after the surfactant; Step 3, add the solution obtained in Step 2 dropwise to the composite masterbatch solution under stirring; Step 4, Extrude the solution obtained in Step 3 and stretch it into silk, Obtain PP wire; step 5, melt another composite masterbatch to obtain a composite masterbatch solution, pass the PP wire through the composite masterbatch solution at a uniform speed, and obtain PP wire coated with a composite masterbatch, and the diameter of the PP wire is 0.001-1mm , preferably 0.5-0.6mm; the speed at which PP wire passes through the composite masterbatch suspension is 0.1-1m / s, preferably 0.4-0.8m / s; step 6, rolling the PP wire obtained in step 5 into a ball, And re-melting, an...
Embodiment 1
[0040] A kind of graphene composite PP fiber, comprises each material of following weight portion:
[0041] Composite masterbatch 25 parts
[0042] PP 90 parts
[0043] Polyethylene glycol 40 parts
[0044] KH550 5 parts.
[0045] Wherein, a kind of composite masterbatch, comprises each material of following parts by weight:
[0046] Graphene 10 parts
[0047] Sodium polyacrylate 10 parts
[0048] 1 part fatty amine salt
[0049] Aluminum oxide 15 parts
[0050] 1 part microcrystalline cellulose
[0051] 10 parts ethanol or acetone
[0052] Silicone 1 part
[0053] 1 plant polyphenol,
[0054] Wherein, the graphene is 3 layers of graphene.
Embodiment 2
[0056] A kind of graphene composite PP fiber, comprises each material of following weight portion:
[0057] Composite masterbatch 10 parts
[0058] PP 90 parts
[0059] Methanol 30 parts
[0060] Sodium fatty alcohol sulfate 2 parts.
[0061] Wherein, a kind of composite masterbatch, comprises each material of following parts by weight:
[0062] Graphene 29 parts
[0063] Sodium polyacrylate 10 parts
[0064] 5 parts fatty amine salt
[0065] Aluminum powder 15 parts
[0066] 2 parts microcrystalline cellulose
[0067] 10 parts ethanol
[0068] Silicone 3 parts
[0069] 1 plant polyphenol,
[0070] Described graphene is 10 layers of graphene.
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