A filler type investment casting wax based on lipophilic micron graphite and preparation method thereof
An investment casting and lipophilic technology, applied in the direction of casting molding equipment, etc., can solve the problems of affecting the reaction accuracy of castings, affecting product quality, poor thermal conductivity, etc., achieve small ash content, meet high dimensional accuracy and high surface quality, The effect of improving thermal conductivity
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[0029] Preferably, the preparation method of lipophilic micron graphite comprises the following steps:
[0030] 1) adding micron graphite into water for ultrasonic dispersion, drying to obtain micron graphite powder;
[0031] 2) adding micron graphite powder into an organic solvent, then adding an oily wetting agent, ultrasonically dispersing, and drying to obtain lipophilic micron graphite.
[0032] Preferably, in step 1) of the method for preparing lipophilic micron graphite, the mass ratio of micron graphite to water is (1-10): (90-99); the temperature of the water is 60-70°C, and the ultrasonic dispersion time is 20 ~30min; the drying temperature is 110~130℃, and the drying time is 12~24h.
[0033] Preferably, in step 1) of the method for preparing lipophilic micron graphite, the micron graphite is micron cryptocrystalline graphite.
[0034] Preferably, in step 2) of the method for preparing lipophilic micron graphite, the mass ratio of micron graphite powder, organic so...
preparation Embodiment 1
[0046] 1) Add 10 parts by mass of cryptocrystalline graphite with a particle size of 30 microns to 90 parts by mass of water (at a temperature of 70°C) for ultrasonic dispersion for 30 minutes to remove acid radical ions and metals remaining during the processing of micron graphite ion, filtered, and baked in an oven at 130°C for 24 hours to obtain micron graphite powder;
[0047] 2) Add 10 parts by mass of micron graphite powder to 90 parts by mass of cyclohexane, add 1 part by mass of paraffin oil, ultrasonically disperse for 60 minutes, filter, and bake in an oven at 90°C for 8 hours to remove the organic solvent , to obtain lipophilic micron graphite.
[0048] Add 10 parts by mass of lipophilic micron graphite obtained by the above preparation method to 90 parts by mass of paraffin, and ultrasonically disperse at 100° C. for 60 minutes to obtain a dispersion. After testing, the dispersion maintains good dispersion stability without delamination after 800 high and low temp...
preparation Embodiment 2
[0050] The preparation method is the same as the preparation example 1 of lipophilic micron graphite, the only difference is that the organic solvent is acetone. After testing, the dispersion maintains good dispersion stability without delamination after 800 high and low temperature cycles (20°C-100°C-20°C).
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