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Surface treatment method of medical metal material

A metal material and surface treatment technology, used in pharmaceutical formulations, medical science, prostheses, etc., can solve the problems of affecting the mechanical properties of the base material, harsh preparation conditions, falling off, etc. effect of life

Active Publication Date: 2018-06-01
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] However, the passivation film on the surface of the medical metal often causes poor bonding between the base alloy and the coating, making the thickness of the anodized film generally less than 1 μm, which cannot meet the requirements of practical applications in many cases; physical / chemical vapor deposition , Ion implantation method and thermal oxidation method need to maintain a certain high temperature in the process of coating preparation, which changes the structure of the substrate and the coating to a certain extent, making the mechanical properties of the titanium alloy substrate significantly worse; physical / chemical vapor phase The preparation conditions required by the deposition and ion implantation methods are relatively harsh, and the cost of modifying titanium alloys is relatively high; the thermal oxidation method consumes a lot of energy and takes a long time to obtain a coating that cannot guarantee uniformity
In the process of preparing the coating by the micro-arc oxidation method, it will greatly affect the mechanical properties of the substrate, especially the fatigue performance, and consume a lot of energy.
As an implant, the biochemical stability of the surface of medical metal materials is particularly important. Unstable coatings and the release of ions will cause many patients to have a series of problems after implant surgery, such as the relationship between the implant and bone tissue. Combined with problems such as slow speed, severe inflammation, loosening or even falling off of the implant, the recovery effect of the surgery cannot meet expectations, etc.

Method used

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Embodiment 1

[0034] This embodiment relates to a surface texture and a preparation method for precisely regulating the surface tribological properties of medical metal materials, including the following steps:

[0035] (1) Mechanically polish the surface of the titanium alloy, and ultrasonically clean it in acetone and alcohol solutions for 20 minutes respectively, and carry out degreasing treatment, refer to figure 1 ;

[0036] (2) Use a 20W ytterbium-doped fiber laser to texture the surface of the material, ablate or induce an artificial surface structure with micron or nanoscale, the basic parameters of the laser are: laser wavelength λ is 1064nm, pulse Frequency 1-100KHz, pulse width τ 1-1000ns; power 1-20W, laser speed 0.1-1.5m / s, lens focal length models: 160nm and 254nm, focal length and sample surface height 150-300mm.

[0037] (3) Use laser micromachining system to process micron-scale texture on the surface of titanium alloy. The diameter of the stacked ring is 10-60um, the thic...

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Abstract

The invention provides a surface treatment method of a medical metal material. The surface treatment method includes the steps of: performing mechanical polishing and oil dirt removal treatment to thesurface of a medical metal material and performing texturing to the surface of the medical metal material with laser so as to ablate or induce surface structures which are in micron / nano-scale and are formed by stacking a plurality of rings. Compared with the prior art, the method has the advantages as follows: 1) through the laser texturing on the surface of the medical metal material, the method can process the material directly in air environment without pollution and noise, the formed patterns being uniform and ordered; 2) friction performance of the medical metal material can be selectively reduced or enhanced, thus effectively broadening the application range of the medical metal material.

Description

technical field [0001] The invention relates to the technical fields of mechanical manufacturing and surface processing of medical devices, in particular to a surface texture and a preparation method for precisely regulating the surface tribological properties of medical metal materials. Background technique [0002] Medical metal materials, such as titanium, titanium alloys and stainless steel, are widely used as biological implants in the field of biomedicine because of their high strength, bending fatigue resistance and good toughness. Commonly used medical metal materials are mainly titanium alloys and stainless steels. However, titanium alloys have poor wear resistance in physiological environments and under load conditions, especially sensitive to adhesive wear. The surface of titanium alloys has biological inertia and poor wear resistance. Damage performance will bring many negative effects during long-term use as a biological implant. Corrosion and wear of other med...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22F3/00C23F4/00A61L27/50A61L27/06
CPCA61L27/06A61L27/50A61L2400/18C22F3/00C23F4/00
Inventor 徐勇张亚东赵世昌张刚强李志鹏任天辉
Owner SHANGHAI JIAO TONG UNIV
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