High-conductivity and low-temperature cured conductive paste and preparation method thereof
A high-conductivity, conductive paste technology, used in cable/conductor manufacturing, equipment for manufacturing conductive/semi-conductive layers, conductive materials dispersed in non-conductive inorganic materials, etc. Industrial application, heating energy consumption and other issues
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Embodiment 1
[0051] A high-conductivity low-temperature curing conductive paste, said high-conductivity low-temperature curing conductive paste, which includes 33 parts by weight of spherical silver powder, 47 parts by weight of flake silver powder, 1 part by weight of carbon nanotubes, 10 parts by weight Bisphenol A epoxy resin in parts by weight, modified imidazole latent curing agent in 1 part by weight, and additives in 8 parts by weight.
[0052] Wherein said addition is DBE, polyvinylpyrrolidone and N-methylpyrrolidone.
[0053] The preparation process parameters are as follows: using a self-rotating and revolving mixer to mix the above materials together to form a slurry; put the initially mixed slurry into a three-roll grinder to grind it into a slurry.
[0054] The above slurry was screen-printed onto an alumina substrate, and then baked at 180° C. for 15 minutes, and then the printed sheet was taken out.
Embodiment 2
[0056] A high-conductivity low-temperature curing type conductive paste, said high-conductivity low-temperature curing type conductive paste, which includes 51 parts by weight of spherical silver powder, 35 parts by weight of flake silver powder, and 2 parts by weight of silver powder with a particle size of 20 nanometers , 0.5 parts by weight of carbon nanotubes, 5.5 parts by weight of liquid novolak epoxy resin, 1 part by weight of acid anhydride curing agent, and 5 parts by weight of additives.
[0057] Wherein said addition is dispersant, polyvinylpyrrolidone and N-methylpyrrolidone.
[0058] The preparation process parameters are as follows: using a self-rotating and revolving mixer to mix the above materials together to form a slurry; put the initially mixed slurry into a three-roll grinder to grind it into a slurry.
[0059] The above slurry was printed onto the alumina substrate by screen printing, and then baked at 180°C for 40 minutes, and then the printed sheet was ...
Embodiment 3
[0061] A high-conductivity low-temperature-curable conductive paste, said high-conductivity low-temperature-curable conductive paste, which includes 80 parts by weight of spherical silver powder, 10 parts by weight of agglomerated silver powder, 2 parts by weight of carbon nano-silver powder deposited nanotubes, 4 parts by weight of epoxy resin, 1 part by weight of amine curing agent, and 3 parts by weight of additives.
[0062] Wherein said addition is ethyl cellulose, DBE and N-methylpyrrolidone.
[0063] The carbon nanotubes deposited with nano-silver powder are made by adding silver nitrate to the aqueous solution of nano-conductive carbon tubes, mixing thoroughly, and filtering the liquid to obtain a filter cake, which is then moved into a sodium bromide solution, and then the solution is adjusted to a wavelength of 150nm to 500nm. Under the condition of light, nano-silver particles deposited on the surface of the carbon nanotubes are formed; the solution after the reacti...
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