Special soldering paste for light-emitting diode (LED) and preparation method thereof
A solder paste and tin powder technology, applied in welding equipment, welding media, manufacturing tools, etc., can solve the problems of reducing LED lighting efficiency and service life, large LED packaging area, affecting the thermal conductivity of the interface, etc., to improve production economic benefits. , The effect of reducing the cost of solder paste and reducing the cost of LED packaging
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[0027] Flux preparation:
[0028] S1. Add KHR-130 rosin crystals, AX-80 fully hydrogenated rosin, maleic acid modified rosin, diethylene glycol hexyl ether, and diethylene glycol dibutyl ether into the high-pressure ultrasonic reactor, and heat up to 125°C. After the solid is completely melted, cool the temperature in the kettle to 60°C and keep it warm, then add glutaric acid, oxalic acid, modified hydrogenated castor oil, tall oil fatty acid, dimer fatty acid, dibromobutyl into the high-pressure ultrasonic reaction kettle in sequence Enediol, 2-ethyl ether azole, 1010 antioxidant, methyl benzotriazole, start the mechanical stirring device and ultrasonic equipment, the speed of the mechanical stirring device is 2000rpm / min, the ultrasonic frequency is 35KHz, and the ultrasonic power is 2000W. The ultrasonic vibration method is continuous vibration. After emulsifying at a temperature range of 60°C for 65 minutes, cool to 25°C;
[0029] S2. The mixture obtained in the step S1 ...
Embodiment 1
[0032] The particle size distribution range of the selected alloy tin powder is 25-45 microns, and the alloy tin powder is composed of 50% tin, 3.5% bismuth, 0.8% antimony, 0.1% nickel and 45.6% lead. Add 10%wt of the above-mentioned flux and 90%wt alloy tin powder into a vacuum stirring tank, and stir evenly to prepare the special solder paste for LED in this embodiment.
[0033] Two aluminum oxide ceramic substrates are selected, namely the methyl plate and the second base plate. The specifications are as follows: the length X width is 12cm X 12cm, and the thickness of the substrate is about 0.38mm.
[0034] Use the obtained LED special solder paste to solder the base plate and the base plate, and connect the upper surface of the base plate and the lower surface of the base plate electrically and mechanically through pulse reflow soldering, and obtain a welding sample after solidification and cooling, and use an X-ray machine to weld the sample The test was carried out, and ...
Embodiment 2
[0036] The selected alloy tin powder has a particle size distribution range of 25 to 45 microns. The alloy tin powder is composed of 40% tin, 7% bismuth, 1.2% antimony, 0.1% copper, and 51.7% lead. Add 9.5% After stirring the above-mentioned soldering flux and 90.5%wt alloy tin powder by wt evenly, the special solder paste for LED in this embodiment is obtained.
[0037] Two aluminum oxide ceramic substrates are selected, namely the methyl plate and the second base plate. The specifications are as follows: the length X width is 12cm X 12cm, and the thickness of the substrate is about 0.38mm.
[0038] Use the obtained LED special solder paste to solder the base plate and the base plate, and connect the upper surface of the base plate and the lower surface of the base plate electrically and mechanically through pulse reflow soldering, and obtain a welding sample after solidification and cooling, and use an X-ray machine to weld the sample The test was carried out, and the void r...
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