Polyurethane material and preparation method thereof
A technology of polyurethane materials and raw materials, applied in the field of polymers, can solve the problems of unresolvable shavings, short service life, general water absorption, etc., to improve the prepolymerization effect and performance, improve the foaming effect, and highlight the catalytic activity. Effect
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[0057] The hardening agent is prepared by mixing and reacting the following raw materials in parts by weight: 10 parts of silica sol, 8-12 parts of ethanol, 2-4 parts of silane coupling agent and 5-8 parts of 1,6-hexanediol diacrylate During the reaction, an appropriate amount of dilute hydrochloric acid or dilute sulfuric acid can be added to provide an acidic hybrid reaction environment. The specific preparation method of the hardening agent includes: firstly adding the silica sol and ethanol in the parts by weight into the three-necked flask, and then adding the silane coupling agent dropwise, dilute hydrochloric acid or dilute sulfuric acid can be used in the reaction process Adjust the pH value, the preferred pH value is adjusted to 3-4, under the condition of stirring, after reacting for 3-6 hours, add the 1,6-hexanediol diacrylate in the weight part, and then add the mixed solution In a single-necked flask, at a temperature of 80-100°C, rotary evaporate until a white so...
Embodiment 1
[0080] A polyurethane material for a highly elastic and antibacterial powder puff, which is made by mixing and reacting the following raw materials in parts by weight:
[0081]
[0082]
[0083] The polyether polyol composition described therein is prepared by mixing and reacting the following raw materials in parts by weight: 10 parts of polytetrahydrofuran ether diol, 5 parts of polyoxypropylene diol, 2 parts of polyoxypropylene triol and tetrahydrofuran-epoxy 1.5 parts of propane copolyether and 4 parts of propylene oxide. The polyether polyol is a polyether polyol with an average molecular weight of 1000-1500 prepared by polyaddition reaction of the raw materials in the above parts by weight.
[0084] The anti-mold additive is prepared by mixing the anti-mold agent and palm wax at a mass ratio of 1:1, and the anti-mold agent is prepared by mixing the following raw materials in parts by weight: dodecyl-α-D glucoside 8 6 parts of isothiazolinone, 2 parts of jasmine ess...
Embodiment 2
[0098] A polyurethane material for a high-elastic antibacterial powder puff, which is made by mixing and reacting the following raw materials in parts by weight:
[0099]
[0100] The polyether polyol composition described therein is prepared by mixing and reacting the following raw materials in parts by weight: 10 parts of polytetrahydrofuran ether diol, 8 parts of polyoxypropylene diol, 5 parts of polyoxypropylene triol and tetrahydrofuran-epoxy 4 parts of propane copolyether and 6 parts of propylene oxide. The polyether polyol is a polyether polyol with an average molecular weight of 2000-3000 prepared from the raw materials in the above weight parts through polyaddition reaction.
[0101]The anti-mold additive is prepared by mixing the anti-mold agent and palm wax at a mass ratio of 1:1, and the anti-mold agent is prepared by mixing the following raw materials in parts by weight: dodecyl-α-D glucoside 10 8 parts of isothiazolinone, 4 parts of jasmine essential oil, 1 pa...
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