A kind of aluminum alloy-alumina composite material and its preparation method and application
A composite material and alumina technology, which is applied in the field of aluminum alloy-alumina composite materials and its preparation, can solve the problems of low manufacturing efficiency of 3D network alumina framework, weak combination of framework and metal matrix, and low sintering yield. Achieve good wave and heat absorption performance, improve production efficiency and yield, and reduce cost
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[0035] The invention provides a method for preparing an aluminum alloy-alumina composite material, comprising the following steps:
[0036] Mix the dry powder with water to obtain alumina slurry;
[0037] molding the alumina slurry by molding or casting to obtain an alumina billet;
[0038] Sintering and drilling the alumina blank to obtain an alumina skeleton;
[0039] Composite the aluminum oxide skeleton and aluminum alloy melt by impregnation method or die casting method to obtain aluminum alloy-alumina composite material;
[0040] Described dry powder comprises the component of following mass percent:
[0041] Aluminum oxide 75%-30%, magnesium oxide 14-30%, titanium oxide 14-30%, dispersant 1%, polyvinyl alcohol 1%.
[0042] In the present invention, unless otherwise specified, the required preparation materials are commercially available products well known to those skilled in the art.
[0043] The invention mixes dry powder with water to obtain alumina slurry. In t...
Embodiment 1
[0078] Taking 100g dry powder to prepare alumina skeleton as an example
[0079] Uniformly mixing alumina, magnesia and titanium oxide powders according to the mass ratio of 75:14:14, milling in a ball mill for 3 hours to obtain a mixed powder with an average particle size of 6-10 μm;
[0080]Dissolve 1g of sodium carboxymethylcellulose and 1g of polyvinyl alcohol in 40mL of water, heat to 90°C, and dissolve to obtain a mixed solution;
[0081] Mix the mixed solution and the mixed powder, and stir for 1 hour under the condition of 3000r / min to obtain alumina slurry;
[0082] Spray the mold with boron nitride release agent, put the alumina slurry into the mold and pressurize at 5MPa, hold the pressure for 1min, and carry out compression molding to obtain a 200mm×200mm square billet; put the square billet into Put it into an oven for drying, control the temperature rise rate to 3°C / min, raise the temperature to 100°C for 1 hour, and obtain an alumina billet;
[0083] Put the a...
Embodiment 2
[0089] Taking 100g dry powder to prepare alumina skeleton as an example
[0090] Uniformly mixing alumina and kaolin powder according to the mass ratio of 69:29, grinding in a ball mill for 3 hours to obtain a mixed powder with an average particle size of 10-15 μm;
[0091] Dissolve 1g of sodium carboxymethylcellulose and 1g of polyvinyl alcohol in 60mL of water, heat to 90°C, and dissolve to obtain a mixed solution;
[0092] Mix the mixed solution and the mixed powder, and stir for 2 hours under the condition of 3000r / min to obtain alumina slurry;
[0093] Spray the mold with a boron nitride release agent, put the alumina slurry into the mold and pressurize at a pressure of 5 MPa, hold the pressure for 30 minutes, and perform compression molding to obtain a 200mm×200mm square billet. Put the square billet into Put it into an oven for hot air drying, control the temperature rise rate to 3°C / min, raise the temperature to 100°C and keep it for 1h to obtain an alumina billet;
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