Preparation method of alkoxy silane
A technology of alkoxysilane and anhydrous alkoxy alcohol, which is applied in the field of preparation of alkoxysilane, can solve the problems of unrecyclable waste, polluted reaction products, low conversion rate of silicon powder, etc., and achieve high heat utilization efficiency, Effect of promoting heterogeneous diffusion and optimizing catalytic effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0055] Add anhydrous ethanol and rectified liquid high boilers into the reactor respectively, the mass ratio of rectified liquid high boilers to absolute ethanol is 1:0.9, control the reaction temperature at 15°C, and the reaction pressure at 0.2MPa. Under the conditions, all the materials are uniformly mixed and reacted to prepare tetraethoxysilane, and the silicon conversion rate is calculated to be 90%, wherein the selectivity of tetraethoxysilane is 97%.
Embodiment 2
[0057] Add absolute ethanol and rectified liquid high boilers into the reactor respectively, the mass ratio of rectified liquid high boilers to absolute ethanol is 1:2, control the reaction temperature -20°C, reaction pressure -0.1MPa, Under the condition of stirring, all the materials were uniformly mixed and reacted to prepare tetraethoxysilane. According to calculation, the silicon conversion rate was 98%, and the selectivity of tetraethoxysilane was 99.2%.
Embodiment 3
[0059] Add anhydrous ethanol and rectified liquid high boilers into the reactor respectively, the mass ratio of rectified liquid high boilers to absolute ethanol is 1:4, control the reaction temperature at 50°C, and the reaction pressure at 0.1MPa. Under the conditions, all the materials are uniformly mixed and reacted to prepare tetraethoxysilane. According to calculation, the silicon conversion rate is 95%, and the selectivity of tetraethoxysilane is 98%.
PUM

Abstract
Description
Claims
Application Information

- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com