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Method for treating VOCs (Volatile Organic Chemicals) and foul gas generated in sucralose production process

A production process, sucralose technology, applied in gas treatment, separation methods, chemical instruments and methods, etc., can solve the problems affecting the normal life activities of surrounding residents, complex recovery process, complex waste gas composition, etc. Simple process and good adaptability

Inactive Publication Date: 2020-06-09
TECHNO (FUJIAN) FOOD INGREDIENTS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the gas elimination method is widely used, but this method has the disadvantages of large equipment investment, high operating costs, and even secondary pollution of the exhaust gas; while the separation method can realize the secondary utilization of resources, but usually requires more Purified solvents can only be obtained through specific processing steps, the recovery process is complex, and the operating costs are also high
[0003] Due to the complex composition of the exhaust gas produced in the production process of sucralose, and its stable performance and refractory degradation, the treatment of the exhaust gas from the production of sucralose has become an obstacle to the production and development of this product
The thermal oxidation treatment of the incinerator used in production not only has the risk of explosion during the combustion process, but also the exhaust gas is difficult to meet the standard. The concentration of VOCs is as high as 5000-6500mg / L, and the concentration of malodorous gas is as high as 350-470mg / L. Secondary pollution, affecting the normal life activities of surrounding residents

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] The amount of waste gas produced during the production of sucralose in this embodiment is 7500m 3 / h, the concentration of VOCs is 6900mg / L, and the concentration of malodorous gas is 482mg / L; VOCs are mainly ethyl acetate, dimethylformamide, methanol, etc., and malodorous gases include ammonia, sulfur dioxide, dimethylamine, hydrogen sulfide Wait. Its processing method steps are as follows:

[0019] (1) The waste gas produced in the above-mentioned sucralose production process is sent into the spray tower, and the sodium hypochlorite solution with a mass concentration of 0.2% is used as a washing liquid for pretreatment and purification. The liquid-gas flow ratio is 0.005. After 5 days of spraying Leaching treatment until the concentration of VOCs in the exhaust gas is 4681mg / L, the concentration of malodorous gas is 372mg / L, the COD concentration of the washing liquid is 1586mg / L, and the concentration of ammonia nitrogen is 52mg / L, and the purified exhaust gas is ob...

Embodiment 2

[0024] The amount of waste gas produced during the production of sucralose in this embodiment is 4500m 3 / h, the concentration of VOCs is 5213mg / L, and the concentration of malodorous gas is 361mg / L; VOCs are mainly ethyl acetate, dimethylformamide, methanol, etc., and malodorous gases include ammonia, sulfur dioxide, dimethylamine, hydrogen sulfide Wait. Its processing method steps are as follows:

[0025] (1) The exhaust gas produced in the above-mentioned sucralose production process is sent into the spray tower, and the Fenton reagent solution formed by the ferrous sulfate+0.1% hydrogen peroxide with a mass concentration of 0.2% is used as a washing liquid for pretreatment Purification, the liquid-gas flow ratio is 0.01, after 5 days of spray treatment, the concentration of VOCs in exhaust gas is 3856mg / L, the concentration of malodorous gas is 216mg / L, the concentration of COD in washing liquid is 1200mg / L, and the concentration of ammonia nitrogen is 38mg / L L, to obtai...

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PUM

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Abstract

The invention discloses a method for treating VOCs (Volatile Organic Chemicals) and foul gas generated in a sucralose production process, which comprises the following steps: firstly, feeding waste gas into a spray tower, and pre-degrading macromolecular organic matters which are difficult to biologically treat originally and foul molecules with high biotoxicity to reduce the biotoxicity of the waste gas; and introducing the waste gas as a nutrient source and a gas source into a wastewater treatment system to quickly degrade the waste gas, thereby implementing simultaneous waste gas treatmentby using the wastewater system. According to the method, chemical reagent aqueous solution pretreatment and microbiological treatment are combined and cooperate with each other, so that the defect that single-stage treatment emission of a chemical solvent does not reach the standard is overcome, the toxicity of the waste gas to organisms is effectively reduced, and up-to-standard emission of VOCsand malodorous gas is realized. The method is simple in treatment process, low in operation cost, wide in applicability and high in waste gas removal rate, the risks of explosion and combustion are completely eradicated by adopting a wet treatment process, and a new way is provided for waste gas treatment in industrial production.

Description

technical field [0001] The invention relates to the technical field of chemical production waste gas treatment, in particular to a treatment method for sucralose production tail gas in industrial production. Background technique [0002] There are two kinds of industrial waste gas treatment methods in the prior art. The one is to eliminate the gas in the waste gas (such as: thermal oxidation, catalytic oxidation, plasma oxidation, biodegradation, photodegradation, etc.); the other is to separate the gas from the waste gas (such as : condensation, membrane separation, adsorption, absorption, etc.). At present, the gas elimination method is widely used, but this method has the disadvantages of large equipment investment, high operating costs, and even secondary pollution of the exhaust gas; while the separation method can realize the secondary utilization of resources, but usually requires more Purified solvents can only be obtained through advanced processing steps, the reco...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D53/44B01D53/48B01D53/54B01D53/78B01D53/84
CPCB01D53/44B01D53/48B01D53/54B01D53/78B01D53/84B01D2257/708Y02A50/20
Inventor 陈靖陆夏莲柯佳怡郑聪陈子昂
Owner TECHNO (FUJIAN) FOOD INGREDIENTS CO LTD
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