A kind of epoxy resin packaging glue and its preparation method and application
A technology of epoxy resin and encapsulation glue, which is applied in the direction of epoxy resin glue, adhesive, non-polymer adhesive additives, etc., and can solve the problems of high crosslinking density, poor moisture resistance, and restrictions on the application of epoxy resin
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preparation example 1
[0079] (1) Take 100 parts of sodium desoil, 3 parts of dodecyltrimethylammonium bromide, and 200 parts of ultrapure water in a beaker, stir them evenly and carry out ultrasonic dispersion. The power of the ultrasonic disperser is set to 600W, and the ultrasonic frequency 40KHz, the ultrasonic time is 20min, and the temperature is set to 60°C; after completion, it is placed in an oven at 80°C for drying treatment, and the product after drying is recorded as α 1 .
[0080] (2) Take the product α of step (1) 1 100 parts, 20 parts of 3', 4'-epoxycyclohexylmethyl 3,4-epoxycyclohexylcarboxylate, 150 parts of xylene, and 0.5 parts of chromium acetylacetonate were placed in a glass cup and sealed, stirred evenly and carried out Ultrasonic dispersion, the power of the ultrasonic disperser is set to 600W, the ultrasonic frequency is 40KHz, the ultrasonic time is 20min, and the temperature is set to 80°C. Toluene solvent, the resulting product is modified montmorillonite, denoted as β ...
preparation example 2
[0082] (1) Take 100 parts of sodium desoil, 3 parts of dodecyltrimethylammonium bromide, and 200 parts of ultrapure water in a beaker, stir them evenly and carry out ultrasonic dispersion. The power of the ultrasonic disperser is set to 600W, and the ultrasonic frequency 40KHz, the ultrasonic time is 20min, and the temperature is set to 60°C; after completion, it is placed in an oven at 80°C for drying treatment, and the product after drying is recorded as α 1 .
[0083] (2) Take the product α of step (1) 1 100 parts, 20 parts of DER-331 epoxy resin, 150 parts of xylene, and 0.5 parts of chromium acetylacetonate were placed in a glass cup and sealed. After stirring evenly, ultrasonic dispersion was performed. The power of the ultrasonic disperser was set to 600W, and the ultrasonic frequency was 40KHz. The time is 20 minutes, and the temperature is set to 80°C. After the dispersion is completed, the above product is added to a vacuum distillation device, and the reaction is c...
preparation example 3
[0085] (1) Take 100 parts of sodium desoil, 3 parts of octadecyltrimethylammonium bromide, and 200 parts of ultrapure water in a beaker, stir them evenly and carry out ultrasonic dispersion. The power of the ultrasonic disperser is set to 600W, and the ultrasonic frequency 40KHz, the ultrasonic time is 20min, and the temperature is set to 60°C; after completion, it is placed in an oven at 80°C for drying treatment, and the product after drying is recorded as α 3 .
[0086] (2) Take the product α of step (1) 3 100 parts, 20 parts of DER-331 epoxy resin, 150 parts of xylene, and 0.5 parts of chromium acetylacetonate were placed in a glass cup and sealed. After stirring evenly, ultrasonic dispersion was performed. The power of the ultrasonic disperser was set to 600W, and the ultrasonic frequency was 40KHz. The time is 20 minutes, and the temperature is set to 80°C. After the dispersion is completed, the above product is added to a vacuum distillation device, and the reaction is...
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