Phosphorus-free nitrogen-free dye-accelerating repairing agent and preparation method thereof
A technology of repairing agent and co-solvent, which is applied in the field of dyeing processing aids, can solve the problems of excessive copper ion content, increase the load of printing and dyeing wastewater and waste gas treatment, and cannot meet the requirements of emission standards at the same time, and achieve good value, good level dyeing and Correction rate, effect of guaranteeing stability and reliability
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Embodiment 1
[0036] a, under normal temperature and pressure, add semi-branched biomass phenol polyoxyethylene ether (N EO =25) 15g, polyethylene glycol oleic acid monoester (600MO) 5g, isomerism decanol polyoxyethylene polyoxypropylene ether sulfate (C 10 EO 5 PO 2 S) 3g, isomerism dodecyl alcohol polyoxyethylene polyoxypropylene ether sulfate (C 12 EO 5 PO 2 S) 1g, 1g of sodium dodecyl diphenyl ether disulfonic acid, 3g of glycerol, 3g of triethylene glycol and 9g of deionized water, heated to 85°C and stirred for 30min to form a stable and uniform solution.
[0037] b. Cool to 60°C under continuous stirring, then add 20 g of dibutyl 1,4-cyclohexanecarboxylate and 15 g of diisononyl 1,2-cyclohexanecarboxylate to the mixture obtained in step a , 2-(acetyl)-1,2,3-tributyl tricarboxylate 20g and then stirred for 50min to form a stable and uniform solution, and cooled to room temperature to obtain the non-phosphorous and nitrogen-free dye-promoting repairing agent 1 #.
Embodiment 2
[0039] a, under normal temperature and pressure, add semi-branched biomass phenol polyoxyethylene ether (N EO =25) 5g, semi-branched biomass phenol polyoxyethylene ether sodium sulfonate (N EO =25) 5g, polyethylene glycol oleic acid monoester (600MO) 5g, isomerism decanol polyoxyethylene polyoxypropylene ether sulfate (C 10 EO 5 PO 2 S) 3g, isomerism dodecyl alcohol polyoxyethylene polyoxypropylene ether sulfate (C 12 EO 5 PO 2 S) 1g, isomeric tridecanol polyoxyethylene polyoxypropylene ether sulfate (C 10 EO 5 PO 2 S) 5g, 1g of sodium dodecyl diphenyl ether disulfonic acid, 3g of glycerol, 7g of triethylene glycol and 10g of deionized water, heated to 85°C and stirred for 30min to form a stable and uniform solution.
[0040] b. Cool to 60°C under continuous stirring, then add 20 g of dibutyl 1,4-cyclohexanecarboxylate and 20 g of diisononyl 1,2-cyclohexanecarboxylate to the mixture obtained in step a , 2-(acetyl)-1,2,3-tributyl tricarboxylate 15g and then stirred for...
Embodiment 3
[0042] a, under normal temperature and pressure, add semi-branched biomass phenol polyoxyethylene ether (N EO =25) 5g, semi-branched biomass phenol polyoxyethylene ether sodium sulfonate (N EO =25) 5g, polyethylene glycol oleic acid monoester (600MO) 15g, isomerism decanol polyoxyethylene polyoxypropylene ether sulfate (C 10 EO 5 PO 2 S) 3g, isomerism dodecyl alcohol polyoxyethylene polyoxypropylene ether sulfate (C 12 EO 5 PO 2 S) 1g, isomeric tridecanol polyoxyethylene polyoxypropylene ether sulfate (C 10 EO 5 PO 2 S) 5g, 1g of sodium dodecyl diphenyl ether disulfonic acid, 3g of glycerol, 2g of triethylene glycol and 10g of deionized water, heated to 90°C and stirred for 15min to form a stable and uniform solution.
[0043] b. Cool to 60°C under continuous stirring, then add 20g of dibutyl 1,4-cyclohexanecarboxylate and 25g of diisononyl 1,2-cyclohexanecarboxylate to the mixture obtained in step a , 2-(acetyl)-1,2,3-tributyl tricarboxylate 5g and stirred for 35min ...
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