Carrier material, bio-adsorbent prepared from carrier material as well as preparation method and application of bio-adsorbent
A biosorbent and carrier material technology, applied in the direction of sustainable biological treatment, chemical instruments and methods, biological water/sewage treatment, etc., can solve the problems that cannot meet the needs of industrial wastewater treatment, limited application sites, weak mechanical properties, etc. Achieve the effect of fast adsorption speed, small environmental impact and good adsorption performance
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[0032] The preparation steps of chitosan / CNT material are as follows:
[0033] S1: Weigh 0.5g of carbon nanotubes (CNT) and disperse them in 20ml of concentrated sulfuric acid, add 2g of sodium nitrite and 5g of diazonium salt p-aminobenzenesulfonic acid, stir and react at 80°C for 2 hours, centrifuge to obtain solids dispersed in 100ml of nitric acid / In concentrated sulfuric acid (1:3), heat to 60°C under reflux and stir for 6 hours, acidify to obtain carboxylated carbon nanotubes;
[0034] S2: Add 0.5g of carboxylated carbon nanotubes and triethanolamine into the reaction bottle containing N,N-dimethylacetamide, stir to disperse evenly; disperse 1ml of methacryloyl chloride in N,N-dimethylacetamide Acetamide was added dropwise to the reaction bottle at 0°C under the protection of nitrogen. After the addition was completed, the reaction bottle was moved to room temperature and stirred for 24 hours, centrifuged, washed and dried;
[0035] S3: Disperse 0.5g of the dried produ...
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