Preparation method of sulfur-doped TiO2 film for water purification system of construction site

A water purification system and construction site technology, applied in chemical instruments and methods, light water/sewage treatment, water/sludge/sewage treatment, etc., can solve problems such as the difficulty of separating and reusing titanium dioxide particles and colloidal catalyst suspensions

A water purification system and construction site technology, applied in chemical instruments and methods, light water/sewage treatment, water/sludge/sewage treatment, etc., can solve problems such as the difficulty of separating and reusing titanium dioxide particles and colloidal catalyst suspensions

CN113385192APending Publication Date: 2021-09-14CHINA MCC17 GRP

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  • Preparation method of sulfur-doped TiO2 film for water purification system of construction site
  • Preparation method of sulfur-doped TiO2 film for water purification system of construction site
  • Preparation method of sulfur-doped TiO2 film for water purification system of construction site

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Embodiment 1

[0034] A sulfur-doped TiO for construction site water purification system 2 The preparation method of the film includes the following steps:

[0035] S1. Synthesis of sol: using a sol-gel process of self-assembly of non-sulfided hydrocarbon surfactants as a pore orienting agent, and using sulfuric acid as a precursor for sulfur and water production;

[0036] S2. Sulfur-doped TiO 2 Preparation of thin films: Preparation of sulfur-doped TiO using borosilicate glass as substrate 2 film;

[0037] S3. Synthesized sulfur-doped TiO 2 Characterization of Thin Films: Measurements Using X-ray Diffractometer to Determine Synthetic Sulfur-Doped TiO 2 The crystal structure of the thin film;

[0038] Photocatalytic activity of S4.MC-LR under visible light irradiation: the solution was prepared in a reactor followed by addition of sulfur-doped TiO 2 film.

[0039] S1 includes the following steps:

[0040] S101. The nonionic surfactant polyoxyethylene (80) sorbitan monooleate (Tween 80)...

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Abstract

The invention discloses a preparation method of a sulfur-doped TiO2 film for a water purification system of a construction site, and belongs to the technical field of water environment treatment. The preparation method comprises the steps of S1, synthesis of sol, specifically, adopting a non-sulfurized hydrocarbon surfactant self-assembled sol-gel process as a pore orientation agent, and taking sulfuric acid as a precursor for preparing sulfur and water; S2, preparation of a sulfur-doped TiO2 film, specifically, preparing the sulfur-doped TiO2 film by using borosilicate glass as a substrate; S3, measuring the characteristics of the synthesized sulfur-doped TiO2 film by adopting an X-ray diffractometer to determine the crystal structure of the synthesized sulfur-doped TiO2 film; and S4, evaluating the photocatalytic activity of MC-LR under visible light irradiation, specifically, preparing a solution in a reactor, and then adding the sulfur-doped TiO2 film. The sulfur-doped TiO2 film has the advantages of high thermal and chemical stability, relatively high photocatalytic activity, low toxicity, low cost and the like.

Description

technical field [0001] The invention relates to the technical field of water environment treatment, in particular to a sulfur-doped TiO used in a construction site water purification system 2 Method for preparing thin films. Background technique [0002] While different membranes such as ultrafiltration and reverse osmosis can remove viruses and bacteria from drinking water, this is not their primary goal. Microbial contaminants in drinking water often occur as a result of sewage discharges, septic tank leaks, and fecal matter entering water bodies from animal feedlot runoff. To protect drinking water from these microorganisms, water providers often add disinfectants, such as chlorine or ozone, to drinking water. However, traditional disinfectants have certain limitations based on water chemistry and the type of microorganisms present. For example, the microorganism Cryptosporidium is highly resistant to traditional disinfection methods. When there are high concentration...

Claims

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Application Information

Patent Timeline
14 Sep 2021
Publication
CN113385192A
IPC
B01J27/02; C02F1/30; C02F101/38; C02F101/34
CPC
B01J27/02; C02F1/30; C02F2305/10; C02F2101/38; C02F2101/34; B01J35/39
Inventors
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