Durable antibacterial composite fabric based on graphene and preparation method thereof
A composite fabric and graphene technology, applied in the field of textile fabrics, can solve problems such as inability to exert antibacterial effect, odor, and reduce fabric air permeability, so as to increase self-cleaning and anti-fouling properties, increase specific surface area, and improve bactericidal performance Effect
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Embodiment 1
[0033] S1: Preparation of the skin-friendly layer
[0034] Cotton fibers are woven to form a skin-friendly layer;
[0035] S2: Preparation of the sweat-absorbing layer
[0036] (1) Impregnating bamboo fibers with 2wt% sodium hydroxide, repeatedly cleaning the bamboo fibers with deionized water to neutrality, and drying; adding the dried bamboo fibers to a water-soluble phenolic resin with a solid content of 33% Soak for 36 hours and dry; under nitrogen protection, keep the temperature at 150 °C for 3 hours of oxidation, then increase the temperature to 600 °C for reaction, cool to 20 °C, add hydrochloric acid, soak for 90 minutes, repeatedly wash with deionized water until neutral, and dry , to obtain modified bamboo fiber;
[0037] (2) Modified bamboo fiber weaving, sewed on the surface of the skin-friendly layer through fiber filaments to form a sweat-absorbing layer;
[0038] S3: Preparation of Antibacterial Layer
[0039] (1) Under the action of ultrasound, add 0.1 mol...
Embodiment 2
[0047] S1: Preparation of the skin-friendly layer
[0048] Cotton fibers are woven to form a skin-friendly layer;
[0049] S2: Preparation of the sweat-absorbing layer
[0050] (1) Impregnating bamboo fibers with 3wt% sodium hydroxide, repeatedly cleaning the bamboo fibers with deionized water to neutrality, and drying; adding the dried bamboo fibers to a water-soluble phenolic resin with a solid content of 36% Soak for 30 hours and dry; under nitrogen protection, keep the temperature at 200 °C for 2 hours of oxidation, then raise the temperature to 800 °C for reaction, cool to 22 °C, add hydrochloric acid, soak for 80 minutes, repeatedly wash with deionized water until neutral, and dry , to obtain modified bamboo fiber;
[0051] (2) Modified bamboo fiber weaving, sewed on the surface of the skin-friendly layer through fiber filaments to form a sweat-absorbing layer;
[0052] S3: Preparation of Antibacterial Layer
[0053] (1) Under the action of ultrasound, add 0.3mol / L a...
Embodiment 3
[0061] S1: Preparation of Modified Bamboo Fibers
[0062] S1: Preparation of the skin-friendly layer
[0063] Cotton fibers are woven to form a skin-friendly layer;
[0064] S2: Preparation of the sweat-absorbing layer
[0065] (1) Impregnating bamboo fibers with 10wt% sodium hydroxide, repeatedly cleaning the bamboo fibers with deionized water to neutrality, and drying; adding the dried bamboo fibers to a water-soluble phenolic resin with a solid content of 40% Soak for 24 hours and dry; under nitrogen protection, keep oxidized at 250 °C for 1 hour, then raise the temperature to 900 °C for reaction, cool to 25 °C, add hydrochloric acid, soak for 30 minutes, repeatedly wash with deionized water until neutral, and dry , to obtain modified bamboo fiber;
[0066] (2) Modified bamboo fiber weaving, sewed on the surface of the skin-friendly layer through fiber filaments to form a sweat-absorbing layer;
[0067] S3: Preparation of Antibacterial Layer
[0068] (1) Under the acti...
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