Preparation method of manganese oxide molecular sieve composite filter material for treating diclofenac in water
A technology of composite filter material and diclofenac, which is applied in chemical instruments and methods, alkali metal compounds, water/sewage treatment, etc., can solve the problems of poor removal effect and high efficiency, and achieve high-efficiency purification of water quality. The preparation method is simple and effective. The effect of removing the effect
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Embodiment 1
[0031] A kind of preparation method of manganese oxide molecular sieve composite filter material for treating diclofenac in water, is characterized in that, carries out as follows:
[0032] (1) Synthesis of manganese oxide molecular sieve, mix potassium permanganate and manganese acetate according to the molar ratio of 2:3 and grind them evenly in a mortar, pour the resulting mixed powder into a capped glass bottle, and place it at 80°C After 4 hours under ambient conditions, the obtained black product was washed 3 times with deionized water and suction-filtered, and finally the obtained material was dried at 80° C. for 12 hours to obtain a manganese oxide molecular sieve.
[0033] (2) Synthesis of amino-modified manganese oxide molecular sieve composite filter material, 1.5g manganese oxide molecular sieve was added into 300mL volume concentration of 50% ethanol aqueous solution, ultrasonic at room temperature for 0.5 hours, 35mL ammonia water was added, and stirred at 60°C fo...
Embodiment 2
[0035] A kind of preparation method of manganese oxide molecular sieve composite filter material for treating diclofenac in water, is characterized in that, carries out as follows:
[0036] (1) For the synthesis of manganese oxide molecular sieve, mix potassium permanganate and manganese acetate according to the molar ratio of 2.5:3 and grind them evenly in a mortar, pour the resulting mixed powder into a capped glass bottle, and place it at 85°C After 5 hours under ambient conditions, the obtained black product was washed 5 times with deionized water and suction-filtered, and finally the obtained material was dried at 85° C. for 12 hours to obtain a manganese oxide molecular sieve.
[0037] (2) Synthesis of amino-modified manganese oxide molecular sieve composite filter material, add 1.5g manganese oxide molecular sieve to 300mL volume concentration of 55% ethanol aqueous solution, ultrasonic at room temperature for 0.5 hour, add 35mL ammonia water, stir at 60°C for 24 hours (...
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