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69 results about "Natural camphor" patented technology

Method for preparing high-purity borneol from lauraceae extract or blumea balsamifera extract

The invention discloses a method for preparing high-purity borneol from a lauraceae extract or a blumea balsamifera extract. The method comprises the following steps: the extracts and secondary alcohol-secondary alcohol aluminum with low boiling point or tertiary alcohol-tertiary alcohol aluminum are heated in a closed environment to evaporate low boiling point secondary alcohol or tertiary alcohol, camphor in the extracts is reduced into borneol or isoborneol, continuous heating is performed in the closed environment to generate borneol aluminum and isoborneol aluminum, continuous heating is performed in the closed environment to dehydrate the isoborneol aluminum, and rearrangement is performed to generate camphene, distilling is performed by using vapor to evaporate camphene and borneol, and camphene and borneol are separated by using one or more of an extraction method adopting saturated hydrocarbon such as petroleum ether and polar solvents such as DMSO, a column chromatography method using saturated hydrocarbon such as petroleum ether and silica gel, and a distillation-sublimation method, and the like. By using the method, the high-purity dextroborneol can be prepared from the auraceae extract, and high-purity levogyration borneol can be prepared from the blumea balsamifera extract. The whole process is continuous, smooth, simple to operate, low in cost, environment-friendly, and high in both purity and yield of the borneol, and facilitates industrial production. The lauraceae extract comprises natural camphor, reduzate, plant borneol camphor, cinnamomum longepaniculatum and cinnamomum burmanni extract.
Owner:闻永举

Method for preparing borneol by using natural camphor powder as raw material

The invention discloses a method for preparing borneol by using natural camphor powder as a raw material. In an alkali metal/anhydrous ethanol reduction system, d-camphor in the natural camphor powder is mainly transformed into d-borneol by using the characteristics of different thermodynamic stabilities of two intermediate products generated by reduction of the d-camphor. The method has the following preparation steps of: refining of the natural camphor powder, asymmetric reduction reaction, reduced pressure distillation and separation of a primary reduced product, secondary reduction of camphor in the primary reduced product, reduced pressure distillation and separation of a secondary reduced product, and obtaining of a target product. The reaction raw materials are natural products of green resources, and relate to comprehensive utilization of spice plants; the conversion rate of the reactants is high and close to 100 percent; because of one-step reaction, the byproducts are few, and the product has high purity; and the method has the advantages of short synthesizing process, low equipment investment, low production cost, high economic benefit, mild reaction condition, short reaction time, low environmental pollution and nearly no environmental pollution.
Owner:HUAQIAO UNIVERSITY

Method for preparing modified PBS copolyester by using camphor alcohol

The invention relates to a method for preparing modified PBS copolyester by using (1S, 3R)-(1)-cis-1, 2, 2-trimethylcyclopentane-1, 3-dimethanol (TCDM). PTS polyester, random PBS copolyester and block PBS copolyester are prepared under the conditions of high temperature and high vacuum by using camphoric acid as a raw material and tetrabutyl titanate as a catalyst. The preparation method comprises the following steps: (1) preparing (1S, 3R)-(1)-cis-1, 2, 2-trimethylcyclopentane-1, 3-dimethanol (TCDM) from camphoric acid; 2) preparing PTS polyester from the TCDM; 3) preparing a random PBS copolyester from the TCDM; 4) preparing the block PBS copolyester from PBS and PTS. The method disclosed by the invention has the advantages that the rigid alicyclic diol is extracted from natural camphor and has high reaction activity, rigidity and better thermal stability. Raw materials are wide in source and low in price; the polyester synthesis process is simple, green and environment-friendly, and is beneficial to industrial production; the prepared modified PBS copolyester material is good in thermal stability, structural and functional diversification is easy to realize, and the performance can be comparable with that of polyester based on a petroleum raw material. The polyester material is degradable, does not cause white pollution, and meets the environmental protection requirement.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

Human resource information clip

The invention discloses a human resource information clip. The human resource information clip comprises a housing, wherein the outer wall of one side of the housing is fixedly provided with a transparent label bag through a bolt; a label is adhered on the inner wall of the transparent label bag; the outer walls of the two sides of the housing are separately connected to a first information boardand a second information board through hinges; two skid-proof stripes are separately arranged on the outer wall of one side of the first information board and the outer wall of one side of the secondinformation board; the outer wall of one side of the first information board and the outer wall of one side of the second information board are fixedly provided with the same locking clip through bolts; and the outer wall of one side of the first information board and the outer wall of one side of the second information board are fixedly provided with two spring clip bases through bolts, and the outer walls of the tops of the two spring clip bases are fixedly provided with two spring clips through bolts. A solid freshener, a ventilating hood and natural camphor balls are arranged, so that offensive odor generated after the information clip is placed for a long time can be eliminated; and meanwhile, the natural camphor balls further have the effects of preventing insects, moths and mildew.
Owner:上海申才科技发展有限公司

Antibacterial insect-resistant furniture paint

InactiveCN107641459AHas antibacterial and antibacterial propertiesGood heat insulationAntifouling/underwater paintsPaints with biocidesSolventPolymerization
The invention relates to the field of coatings, and particularly relates to antibacterial insect-resistant furniture paint. The antibacterial insect-resistant furniture paint is prepared from the following raw materials in parts by weights: 45 to 55 parts of waterborne polyurethane acrylates, 20 to 30 parts of dipentaerythritol hexaacrylate, 5 to 8 parts of natural camphor oil, 2 to 8 parts of nano titanium dioxide photocatalyst, 5 to 10 parts of solvents, 10 to 15 parts of algae soil, 2 to 5 parts of photoinitiator, 0.1 to 0.4 part of graphene, 0.1 to 0.3 part of polymerization inhibitor, 0.1to 0.3 part of anti-greening agent, 0.1 to 0.4 part of anti-foaming agent, 0.3 to 0.6 part of leveling agent, and 0.1 to 0.2 part of anti-settling agent. In a production process, the waterborne polyurethane acrylates, 50 percent of solvents and algae soil, the graphene, the polymerization inhibitor, the leveling agent and the anti-foaming agent are mixed and evenly stirred; the nano titanium dioxide photocatalyst, remaining 50 percent of solvents, the anti-greening agent and the anti-settling agent are continuously stirred until the components are distributed uniformly; then adding an accelerating agent and the photocatalyst to obtain the antibacterial insect-resistant furniture paint. The product has a stable structure and has excellent formaldehyde scavenging performance and bacteriostatic antimicrobial performance; meanwhile, adhesive power of the product is more firm, and scrub-resistant, crack-resistant, and heat insulation effects are good.
Owner:CHENGDU NASHUO TECH
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