Conductivity hydrogels composite material sensitized to humidity variation
A conductive hydrogel and composite material technology, applied in the analysis of materials, the use of electrical devices, the use of electromagnetic means, etc., can solve the problems of sudden changes in electrical properties, poor dimensional stability, and small resistance changes, and achieve a large degree of design freedom. Effect
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Embodiment 1
[0027] For the preparation of carbon nanotube / polyacrylamide composite materials and devices, add 100 mL of deionized In the water, nitrogen gas was introduced to remove the oxygen in the water, and the carbon nanotubes were uniformly dispersed in the water to form a stable suspension after ultrasonic oscillation for 4 hours; 0.133g of N, N methylenebisacrylamide and 160mg of tetramethylethylenediamine were added and 40mg of ammonium persulfate, after mixing evenly, pour it into a pre-laid container made of porous nickel foam as an electrode, seal it and have a cross-linking reaction at room temperature, take out the cross-linked gel after 1h, and put it under nitrogen Soak in saturated distilled water for 24 hours to wash away unreacted components to obtain a soft and elastic carbon nanotube / polyacrylamide gel composite material. After taking it out, the electrode is trimmed to prepare a humidity sensor device.
[0028] The resistivity when it is wet and saturated is 31500Ωcm...
Embodiment 2
[0030]Weigh 3.2 grams of conductive carbon black and 8 grams of monomeric acrylic acid, add 30 ml of water and 0.1 gram of surfactant sodium lauryl sulfate after mixing, stir evenly and put it into an ultrasonic oscillator to vibrate for 2 hours to achieve uniform mixing. At room temperature, after adding 0.2 grams of N, N methylenebisacrylamide, 0.4 grams of potassium persulfate and 0.4 grams of sodium sulfite, pour it into a cylindrical mold with a nickel sheet at one end and lead wires as electrodes. In the process, seal the mold with the other end of the same electrode, and then put it in an 80°C water bath to react for 120 minutes; after the reaction, take out the shaped gel composite material and trim the electrode to obtain a conductive hydrogel composite material and devices.
[0031] Its resistivity in the wet state is 25000Ωcm, and the resistivity in the dry state is 100Ωcm, which is 250 times lower, which is closely related to the close connection of the conductive ...
Embodiment 3
[0033] Weigh 20 g of polyvinyl alcohol (PVA) (polymerization degree 1750, alcoholysis degree 99%), add 160 mL of deionized water, stir and heat up to completely dissolve, add 20 g of conductive carbon black, and cool to room temperature after ultrasonic oscillation for 3 hours; Add 20g of formaldehyde solution with a mass concentration of 37% as a crosslinking agent, 50g of a sulfuric acid solution with a mass concentration of 35% as a catalyst, and 1g of a surfactant. After uniformly stirring in a constant temperature water bath at 35°C, pour it into the prepared In a cylindrical mold with a nickel sheet at one end and a wire drawn out as an electrode, the sealed mold with the other end of the same electrode is cured in an oven at 60 ° C for 4 to 6 hours. Soluble PVA forms water-insoluble polyvinyl formal (PVFM) due to partial cross-linking, with a degree of acetalization of 60%. Take out and wash off unreacted formaldehyde and sulfuric acid, and prepare a black, elastic elect...
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