Ultrathin section steel structure fire-resisting paint and preparation thereof
A technology for fire-resistant coatings and steel structures, which is used in fire-resistant coatings, coatings, and devices for coating liquids on surfaces, etc. injuries, etc.
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Embodiment 1
[0070] 1. Preparation of acrylic bulk hybrid emulsion
[0071] (1) Monomer components: dissolve 16g of oily methyl methacrylate copolymer resin (molecular weight 40000), 3g bisphenol A type epoxy resin (molecular weight 350~400), in 4g methacrylic acid, 25g butyl acrylate And in the mixed monomer of 30g methyl methacrylate, and add the auxiliary solvent propylene glycol butyl ether 20g that increases system stability.
[0072] Initiator Components: Dissolve 0.1 g of potassium persulfate in 20 g of deionized water.
[0073] (2) Add 0.1g sodium bicarbonate, 0.5g sodium dodecylbenzenesulfonate, 3g polyoxyethylene nonylphenol ether acrylate, 10g nonylphenol ether acrylate to a four-neck flask equipped with a thermometer, agitator, and reflux condenser. Dissolve phenol polyoxyethylene ether in 120g deionized water, stir evenly, blow nitrogen for 20 minutes, add 0.5g tert-hexadecanyl mercaptan, 1g methacrylic acid, 1g hydroxyethyl acrylate, 8g butyl acrylate, 10g methyl For methyl...
Embodiment 2
[0084] 1. Preparation of acrylic bulk hybrid emulsion
[0085] (1) Monomer component: monomer component: 10g oily methyl methacrylate copolymer resin, 10g oily butyl methacrylate and acrylonitrile copolymer resin, 3g alkyd resin, 0.2g benzoyl peroxide, 0.3 primary dodecyl mercaptan was dissolved in the mixed monomer of 4g of acrylic acid, 25g of butyl acrylate and 30g of acrylonitrile, and 18g of co-solvent propylene glycol methyl ether was added to increase the stability of the system.
[0086] Initiator Components: Dissolve 0.1 g of ammonium persulfate in 20 g of deionized water.
[0087] (2) In a four-necked flask equipped with a thermometer, a stirrer, and a reflux condenser, add 0.1g sodium bicarbonate, 0.5g sodium lauryl sulfate, 3g polycondensate of succinic acid and glycidyl methacrylate , 5g of alkylphenol ethoxylates, 5g of nonylphenol ethoxylates, dissolved in 120g of deionized water, stirred evenly, passed nitrogen for 20 minutes, added 0.2 primary dodecyl mercapt...
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