Method for preparing spirit flavoring wine or spirit flavour liquid mainly with fragrance

A seasoning wine and seasoning liquid technology, which is applied in the field of liquid fermentation to prepare aroma-based liquor seasoning wine or seasoning liquid, can solve the problems of poor palatability of feed, high technology and energy consumption, and poor sales prospects, etc. Coordination, strong natural sense of wine body, and the effect of avoiding secondary environmental pollution

Inactive Publication Date: 2009-06-17
SICHUAN YINFAN BIOTECH LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Sichuan Province, as a major wine-making province in China, has accounted for more than 67% of the country's total output of raw wine. In recent years, except for a few large-scale wine-making enterprises that have dealt with the "four waters" of waste, such as: using waste grains to produce white carbon black, Reuse of evaporated waste water, as well as biochemical treatment with anaerobic technology; or use waste and waste liquid to produce DDGS high-protein feed, but this method is due to high technology and energy consumption, poor feed palatability, poor sales prospects, and liquor companies basically give up ; There are also enterprises that use yellow water and other "four waters" to anaerobically produce biogas, but a large number of small and medium-sized enterprises basically discharge directly without treatment

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] The preparation of embodiment one fermentation medium

[0038] According to the weight ratio, mix the yellow water, waste liquid, tail water and pot bottom water produced in the production of solid-state fermented liquor at a ratio of 7:1:1:1, and then add 1.5% sodium acetate and dihydrogen phosphate to the mixed solution. Potassium 0.04%, adjust the pH to 6.5-7.0 with ammonium bicarbonate, sterilize at 105°C for 20 minutes, and finally add 2% (V / V) 95° ethanol.

[0039] The ratio of carbon to nitrogen in the fermentation medium is 1:1.2-1.9.

Embodiment 2

[0040] The liquid state fermentation of embodiment two composite strains

[0041] Into the fermentation medium, 20% of the composite bacterial seed liquid is added according to the volume ratio, under the anaerobic fermentation conditions of 34-37 DEG C and pH 6.5-7.0, and cultured for 7-13 days to obtain the fermentation liquid.

[0042] During the fermentation period, the self-produced air pressure of the fermenter is kept at 0.25-0.30Mpa.

[0043] The composite strains include Clostridium butyricum with a strain number of SICC1.91, Clostridium krusei with a strain number of SICC1.13 and Acetobacter pasteurianus with a strain number of SICC1.2.

[0044] The culture medium of described three kinds of strains and compound strains is:

[0045] 1. Slant culture medium: sodium acetate 0.5%, dipotassium hydrogen phosphate 0.04%, magnesium sulfate 0.02, ammonium sulfate 0.05%, yeast extract 0.5%, calcium carbonate 1%, agar 2%;

[0046] 2. Seed medium: sodium acetate 0.5%, dipotas...

Embodiment 3

[0051] The extraction of embodiment three fermented liquid

[0052] After the fermentation is finished, put the fermented liquid in a three-legged centrifuge, and continuously feed and centrifuge under the condition of 1450r.p.m. The sludge is recovered for recycling. The centrifuged liquid is adjusted to pH 3.5-4.0 with food-grade sulfuric acid, and then heated Denature the free protein at 80°C, then add 20% (V / V) 72° base wine to quickly settle the impurities, and at the same time turn on the air compressor to ventilate and deodorize, and use a filter centrifuge to remove the impurities after the odor is gone , the obtained centrifugate is concentrated by double-effect vacuum distillation, and then fractionated and refined by a rectification tower to become a three-stage fractionated liquid: an alcohol section, a water phase section, and a post-distillation section; 10%, 1% of Aroma Yeast and 20% of 72° base wine, stirred intermittently at 34°C, that is, stirred at 120r.p.m ...

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PUM

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Abstract

The invention discloses a method for preparing a spirit flavoring spirit or a spirit flavoring liquor mainly aroma through liquid state fermentation and biological esterificaiton by using wastes produced from solid fermentation spirit production as culture mediums of composite bacteria. The composite bacteria comprise clostridium butyricum with a bacteria number of SICC1. 91, clostridium koseri with a bacteria number of SICC1. 13 and clostridium barati with a bacteria number of SICC1. 2; the composite bacteria fermentation mediums comprise yellow water, tail water, lees solution and pot-bottom water with a weight ratio of 7-8: 0. 5-1: 0. 5-1: 0. 5-1. Sodium acetate 1. 5and dibasic potassium phosphate 0. 04are added in the mixture solution, and ammonium bicarbonate is added to adjust pH value to 6. 5-7. 0, 95 degree ethanol 2 0s added after sterilization, then the mixture solution is sterilized at temperature 105 DEG C for 20min. The invention solves the pollution problem of the wastes to the water environment from the solid spirit production process. The added spirit body is more coordinate, which prevents the defect that the addition of monomer product easily generates float fragrant flavor. The spirit has strong nature feeling, and the recovered bacterial sludge and other residual nutritive matters can be recycled in the fermentation process and avoid secondary environment pollution.

Description

technical field [0001] The invention relates to a preparation method of liquor seasoning wine or seasoning liquid used for edible liquor. Specifically, the invention relates to a method of using bioengineering technology, using solid-state fermented wine-making waste as raw material, and preparing aroma liquor through liquid-state fermentation. The method of seasoning wine or seasoning liquid based on liquor. Background technique [0002] Chinese liquor has been produced for hundreds of years, but most still follow the ancient and traditional production process, which is completely different from the production methods of foreign whiskey, brandy, gin, vodka and other distilled spirits. [0003] The current production status of commercial liquor mainly includes the following types: 1. The wine steamed by removing the head and picking the tail, generally at 50° to 70°, initially combined to form the original wine with a basically balanced aroma, and stored for half a year or a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C12G3/02
Inventor 黄建林李平汪淑容季良威
Owner SICHUAN YINFAN BIOTECH LTD
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