Aqueous emulsion formulated by abamectin and indoxacarb and preparation method thereof
A technology of abamectin and indoxacarb, which is applied in the field of compound water emulsion and its preparation, can solve the difficulty of making water emulsion and other problems, and achieve the effect of avoiding adverse effects
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Embodiment 1
[0032] 0.5 grams of 92% Abamectin and 15 grams of 95% indoxacarb were dissolved in 22 grams of mixed solvent containing N-octylpyrrolidone and Solvesso 150. After the solution was transparent, 1 gram of BHT, 2 grams of poly (12-Hydroxystearic acid) polyoxyethylene ether block copolymer is emulsified into dispersed phase, under high shear (5000-10000rpm), slowly adds to the polyoxyethylene ether containing 3 grams of tristyrylphenol polyoxyethylene ether (Nongru 600#), 0.3 g of silicone defoamer, 4 g of ethylene glycol, 0.1 g of sodium benzoate, 0.25 g of xanthan gum, and 51.85 g of water in the continuous phase (aqueous phase), continue to shear for a few minutes after adding. The viscosity of the obtained water emulsion is 200cP (measured by ROOKFIELD DV-+Proviscometer No. 2 rotor speed 60, the same as the following examples), and the particle size is 0.3-5 microns (measured by the Malvern laser particle size distribution analyzer, the same as the following examples).
[0033...
Embodiment 2
[0036] 2.0 grams of 92% Abamectin and 13 grams of 95% indoxacarb were dissolved in 25 grams of mixed solvent containing diethyl phthalate and Solvsso 200. After the original drug was completely dissolved and became transparent, 1 Gram BHA, 1.5 grams of nonionic surfactant polyisosuccinic anhydride-polyethylene glycol copolymer are emulsified into dispersed phase (oil phase), and under high shear (5000-10000rpm), add to containing 4 grams of nonylphenol In the continuous phase composed of polyoxyethylene ether (OP-20, HLB=16), 0.3 gram of silicone defoamer, 4 gram of propylene glycol, 0.1 gram of formaldehyde, 0.25 gram of gelatin and 48.85 gram of water, after adding the oil phase Continue shearing for several minutes to obtain an emulsion in water with a viscosity of 185 cP and a particle size of 0.25-4 microns.
[0037] Change the feeding method, add above-mentioned 57.5 grams of continuous phases under high shear (5000-10000rpm), add in 42.5 grams of dispersed phases, after...
Embodiment 3
[0040] 5.0 grams of 92% Abamectin and 11 grams of 95% indoxacarb are dissolved in 25.5 grams of mixed solvent containing JEFFSOL AG 1723 (alkylene carbonate, produced by Huntsman Company) and Solvesso200, at <60 degrees Celsius temperature Under heating slightly, after the original drug is completely dissolved into a transparent state, add 1 gram of BHT, 2.5 grams of nonionic surfactant castor oil polyoxyethylene ether (By-125) to emulsify into a dispersed phase (oil phase). Under high shear (5000-10000rpm), the disperse phase is added to containing 3.5 grams of anionic surfactant tristyrylphenol polyoxyethylene ether phosphate (neutralized with triethanolamine, Soprophor FL is produced by Rhdia Company), 0.3 grams Silicone defoamer, 4 grams of polyethylene glycol, 0.1 gram of sorbic acid, 0.25 gram of polyvinyl alcohol, 1 gram of phosphoric acid and 45.85 grams of water in the continuous phase (water phase), after the oil phase is added, continue to high shear After cutting f...
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