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Face-centred cubic structure Ti3Si nano particles and preparation method thereof

A nanoparticle and face-centered cubic technology is applied in the field of face-centered cubic Ti3Si nanoparticles and their preparation, which can solve the problems of long production cycle, environmental pollution, complex process, etc., and achieves low energy consumption, wide application prospects and simple process. Effect

Inactive Publication Date: 2010-08-04
无锡润鹏复合新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the current research has many problems such as complex process, long production cycle, high energy consumption, and a certain degree of pollution to the environment, so the application is greatly restricted, and titanium-silicon alloy nanomaterials have not been used Many natural advantages are fully used by human beings

Method used

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  • Face-centred cubic structure Ti3Si nano particles and preparation method thereof
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  • Face-centred cubic structure Ti3Si nano particles and preparation method thereof

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Experimental program
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Effect test

Embodiment 1

[0017] According to the molar ratio of 3:1, take respectively 20 g of analytically pure grade titanium powder (300 mesh) and 3.89 g of silicon powder (300 mesh), put them into the ball mill jar of the planetary high-energy ball mill after mixing them evenly in a mortar, and pour them into the ball mill jar. Add 10ml of alcohol as the liquid medium of the ball mill, evacuate the ball mill tank, pass in Ar (argon gas), the ventilation rate is 0.5L / min, and use three kinds of steel balls with diameters of 10mm, 6mm and 4mm respectively under 0.2Mpa 50 pieces each, ball mill the mixture for 12 hours, the voltage of the ball mill is 110V, and the speed of the ball mill is 200rad / min; after ball milling, put the mixture into a vibrating dryer, and raise the temperature to 50°C at a heating rate of 5°C / min Finally, vibrate and dry for 60 minutes to completely remove alcohol, then cool naturally to room temperature, and pass through a 300-mesh sieve to obtain the face-centered cubic Ti...

Embodiment 2

[0020] Weigh respectively 20 g of analytically pure grade titanium powder (300 mesh) and 4.67 g of silicon powder (300 mesh) according to the molar ratio of 3: 1.2, put them into the ball mill jar of the planetary high-energy ball mill after mixing them evenly in a mortar, and pour them into the ball mill jar Add 10ml of alcohol as the liquid medium of the ball mill, evacuate the ball mill tank, pass in Ar (argon gas), the ventilation rate is 0.5L / min, and use three kinds of steel balls with diameters of 10mm, 6mm and 4mm respectively under 0.2Mpa 50 pieces each, ball mill the mixture for 12 hours, the voltage of the ball mill is 110V, and the speed of the ball mill is 200rad / min; after ball milling, put the mixture into a vibrating dryer, and raise the temperature to 50°C at a heating rate of 5°C / min Finally, vibrate and dry for 60 minutes to completely remove alcohol, then cool naturally to room temperature, and pass through a 300-mesh sieve to obtain the face-centered cubic ...

Embodiment 3

[0023] Weigh respectively 20 g of analytically pure grade titanium powder (300 mesh) and 5.83 g of silicon powder (300 mesh) according to the molar ratio of 3: 1.5, put them into the ball mill jar of the planetary high-energy ball mill after mixing them evenly in a mortar, and pour them into the ball mill jar Add 10ml of alcohol as the liquid medium of the ball mill, evacuate the ball mill tank, pass in Ar (argon gas), the ventilation rate is 0.5L / min, and use three kinds of steel balls with diameters of 10mm, 6mm and 4mm respectively under 0.2Mpa 50 pieces each, ball mill the mixture for 12 hours, the voltage of the ball mill is 110V, and the speed of the ball mill is 200rad / min; after ball milling, put the mixture into a vibrating dryer, and raise the temperature to 50°C at a heating rate of 5°C / min Finally, vibrate and dry for 60 minutes to completely remove alcohol, then cool naturally to room temperature, and pass through a 300-mesh sieve to obtain the face-centered cubic ...

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Abstract

The invention discloses face-centred cubic structure Ti3Si nano particles and a preparation method thereof. In the method, titanium powder and silicon powder are used as main materials, argon is used as protective gas, alcohol is used as liquid medium for ball milling, a planetary high-energy ball mill and a vibration drier are used as main production devices, and a mechanical alloying method is used to prepare the face-centred cubic structure Ti3Si nano particles. The method has the advantages of simple technology, easily-controlled parameters, short production cycle, low energy consumption and no environment pollution, and is fit for industrialization production. The face-centred cubic structure Ti3Si nano particle has the advantages of small diameter of 15-120nm, low density, high strength, high temperature resistance, oxidation resistance, good electrical conductivity and heat conduction, and the like, and has wide application prospect and huge potential economic benefits in engineering technology, space technology, national defense industry, micro-electronics and other fields.

Description

technical field [0001] The present invention relates to nano-titanium silicon compound, specifically, a face-centered cubic structure Ti 3 Si nanoparticles and methods for their preparation. Background technique [0002] Titanium-silicon alloys have attracted increasing attention due to their good casting properties and mechanical properties. Metastable materials such as nanocrystalline and amorphous titanium-silicon alloys have low density, high strength, high temperature resistance, oxidation resistance, It is expected to be more widely used in important fields such as microelectronics, aerospace, and national defense due to its excellent electrical and thermal conductivity. At present, the research on titanium-silicon alloy nanomaterials mainly focuses on Ti 5 Si 3 aspect, especially for adding Ti 5 Si 3 The changes of thermal expansion coefficient, Young's modulus, hardness, creep strength, fracture toughness, etc. of the latter alloy are deeply discussed. However,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B33/06B82B3/00
Inventor 李长生吴琼唐华
Owner 无锡润鹏复合新材料有限公司
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