Preparation method of hercynite
A technology of iron-aluminum spinel and iron salt, which is applied in the field of preparation of iron-aluminum spinel, can solve the problems of non-compact structure, high sintering temperature of iron-aluminum spinel, low content of iron-aluminum spinel, etc., and achieve internal Compact structure, shortened reaction time, fully and evenly reacted effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0028] Example 1
[0029] A method for preparing iron-aluminum spinel, the steps are as follows:
[0030] 1) Mix aluminum nitrate and ferric nitrate at a molar ratio of 2:1 and dissolve them in ethanol to make a mixed solution with a concentration of 1 mol / L for use;
[0031] 2) Add ammonia water dropwise to the mixed solution prepared in step 1 while stirring for neutralization until the pH of the mixed solution is 7, and precipitation is generated during the neutralization process;
[0032] 3) Filter out the precipitate in step 2, wash with distilled water, add ethylene glycol for dispersion, and then dry it for use;
[0033] 4) The dried precipitate in step 3 is calcined at 300°C-800°C for 1-3h, then 5% of the total weight of the precipitate and 1.6% graphite powder are added and mixed thoroughly. , Use cold isostatic pressing to form a compact for use;
[0034] 5) The briquettes prepared in step 4 are sintered under a vacuum condition of 1400°C for 4 hours, and after natural cooling...
Example Embodiment
[0035] Example 2
[0036] A method for preparing iron-aluminum spinel, the steps are as follows:
[0037] 1) Mix aluminum chloride and ferric chloride at a molar ratio of 2:1 and dissolve them in distilled water to make a mixed solution with a concentration of 1 mol / L for use;
[0038] 2) Add sodium hydroxide solution dropwise to the mixed solution prepared in step 1 while stirring for neutralization until the pH of the mixed solution is 7, and precipitation is generated during the neutralization process;
[0039] 3) Filter out the precipitate in step 2, wash with distilled water, add absolute ethanol for dispersion, and then dry it for use;
[0040] 4) The dried precipitate in step 3 is calcined at 300°C-800°C for 1-3h, then 3% of the total weight of the precipitate and 1% graphite powder are added and mixed thoroughly. After that, cold isostatic pressing is used to form compacts for use;
[0041] 5) The briquettes prepared in step 4 are sintered at 1550°C under argon protection for 3 ...
Example Embodiment
[0042] Example 3
[0043] A method for preparing iron-aluminum spinel, the steps are as follows:
[0044] 1) Mix aluminum sulfate and ferrous sulfate according to the molar ratio of aluminum ion to iron ion 2:1 and dissolve them in distilled water to make a mixed solution with a concentration of 1mol / L;
[0045] 2) Add potassium hydroxide solution dropwise to the mixed solution prepared in step 1 while stirring for neutralization until the pH of the mixed solution is 7, and precipitation is generated during the neutralization process;
[0046] 3) Filter out the precipitate in step 2, wash with distilled water, add ethylene glycol for dispersion, and then dry it for use;
[0047] 4) The dried precipitate in step 3 is calcined at 300°C-800°C for 1-3h, and then 1% polyethylene glycol and 2.5% graphite powder of the total weight of the precipitate are added, and after mixing well, Press cold isostatic pressing into a compact for use;
[0048] 5) The briquettes prepared in step 4 are sintere...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap