Method for producing pure sugar solution, and method for producing chemical product
A manufacturing method and solution technology, applied in the production of sugar, chemical instruments and methods, sugar production, etc., can solve the problems of low removal efficiency, hindering the boiling point of substances, input large energy, etc., and achieve the effect of improving fermentation production efficiency
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[0144] Hereinafter, in order to demonstrate the manufacturing method of the refined sugar aqueous solution of this invention in more detail, an Example is given and demonstrated. However, the present invention is not limited to these examples.
reference example 1)
[0145] (Reference Example 1) Analysis method of monosaccharide concentration
[0146] The concentration of monosaccharides (glucose and xylose) contained in the obtained aqueous sugar solution was quantified by comparing it with a standard sample under the HPLC conditions shown below.
[0147] Column: Luna NH 2 (manufactured by Phenomenex Corporation)
[0148] Mobile phase: ultrapure water: acetonitrile = 25:75 (flow rate 0.6mL / min)
[0149] Reaction solution: no
[0150] Detection method: RI (differential refractive index)
[0151] Temperature: 30°C.
reference example 2)
[0152] (Reference example 2) Analytical method for the concentration of fermentation inhibitors
[0153] Quantification of furanic fermentation inhibitors (HMF, furfural) and phenolic fermentation inhibitors (vanillin, acetylvanillin) contained in sugar aqueous solution by comparing with standard samples under the HPLC conditions shown below .
[0154] Column: Synergi HidroRP 4.6mm×250mm (manufactured by Phenomenex)
[0155] Mobile phase: acetonitrile-0.1%H 3 PO 4 (flow rate 1.0mL / min)
[0156] Detection method: UV (283nm)
[0157] Temperature: 40°C.
[0158] Organic acid fermentation inhibitors (acetic acid, formic acid) contained in the sugar aqueous solution were quantified by comparing with standard samples under the HPLC conditions shown below.
[0159] Column: Shim-Pack SPR-H and Shim-Pack SCR101H (manufactured by Shimadzu Corporation) in series
[0160] Mobile phase: 5mM p-toluenesulfonic acid (flow rate 0.8mL / min)
[0161] Reaction solution: 5mM p-toluenesulfonic...
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