Iron-containing hydrated alumina molded matter and preparation method thereof, and iron-containing alumina molded matter and applications of iron-containing hydrated alumina molded matter and iron-containing alumina molded matter
A technology of hydrated alumina and moldings, which is applied in metal/metal oxide/metal hydroxide catalysts, chemical instruments and methods, chemical/physical processes, etc., and can solve problems such as unfavorable health of operators and unfavorable environmental protection. Achieve environmental protection, reduce the impact on the health of operators, and reduce the amount of acid gas
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Embodiment 1
[0078] With stirring, 10.0g ferric chloride (FeCl 3 ·6H 2 O) Dissolve in 90mL deionized water to obtain ferric chloride solution. 100.0g of pseudoboehmite powder (purchased from Sinopec Catalyst Changling Branch, dry basis content of 69.5% by weight), 4.0g of methylcellulose (purchased from Zhejiang Haishen Chemical Co., Ltd.), 3.0g of Sesame powder Mix well with the above ferric chloride solution. The resulting mixture is fed into an extruder and extruded to obtain a wet strip. The extruded wet strip was placed in an oven and dried at 150° C. for 12 hours, so as to obtain the iron-containing hydrated alumina molding according to the present invention. The radial crushing strength, water absorption rate and δ value of the obtained moldings were measured, and the results are listed in Table 1.
Embodiment 2
[0086] (1) In a 2L reaction tank, add 2000mL of aluminum sulfate solution and sodium metaaluminate solution (Al 2 o 3 content of 200g / L, caustic coefficient of 1.58) for precipitation reaction, the reaction temperature is 50°C, the pH value is 6.0, and the reaction residence time is 15 minutes; the obtained slurry is filtered with a vacuum filter. Add 20L of deionized water (at a temperature of 40±5°C) to the filter cake to rinse the filter cake for about 60 minutes. Add the washed filter cake to 1.5L deionized water and stir to form a slurry, then pump the slurry into the spray dryer for drying, control the outlet temperature of the spray dryer within the range of 100-110°C, and the material drying time for 2 minutes to obtain hydrated alumina, where, Al 2 o 3 The content is 63% by weight, and it is determined to be amorphous by XRD analysis.
[0087] (2) With stirring, 6.0g ferric chloride (FeCl 3 ·6H 2 O) Dissolve in 95mL deionized water to obtain ferric chloride solu...
Embodiment 3
[0089] At a temperature of 60°C, with stirring, 16.0 g of ferric chloride (FeCl 3 ·6H 2 O) Dissolve in 95mL deionized water to obtain ferric chloride solution. 60.0g of pseudo-boehmite (purchased from Sinopec Catalyst Changling Branch, with a dry basis content of 69.5% by weight), 40.0g of gibbsite (purchased from Guangxi Pingguo Aluminum Company, with a dry basis content of 64.5% by weight %), 1.0g methylcellulose (purchased from Zhejiang Haishen Chemical Co., Ltd.), 2.0g hydroxypropyl methylcellulose (purchased from Zhejiang Haishen Chemical Co., Ltd.), 3.0g scallop powder and the above ferric chloride The solution was stirred evenly. The resulting mixture is fed into an extruder and extruded to obtain a wet strip. The obtained wet strip was placed in an oven and dried at 80° C. for 12 hours, so as to obtain the iron-containing hydrated alumina shaped article according to the present invention. The radial crushing strength, water absorption rate and δ value of the obtain...
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