Method for preparing blue titanium dioxide
A titanium dioxide and blue technology is applied in the field of inorganic nano-photocatalyst materials to achieve the effects of simple method, high yield and good optical performance
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0042] Example 1
[0043] The blue titanium dioxide of this example was prepared as follows:
[0044] a. Dissolve 2.32 grams of anhydrous titanium tetrachloride in 5ml of absolute ethanol in an ice bath to prepare a 37% ethanol solution of titanium tetrachloride by mass;
[0045] b. At room temperature, add 2ml of titanium trichloride to 5ml of absolute ethanol to obtain mixed solution A, and then add 0.3g of sodium fluoride powder to mixed solution A to obtain mixed solution B. Titanium trichloride and fluoride The molar ratio of sodium powder is 2:1;
[0046] c. At room temperature, add 0.18 ml of the ethanol solution of titanium tetrachloride obtained in step a to the mixed solution B obtained in step b to obtain mixed solution C, wherein the molar ratio of titanium tetrachloride to titanium trichloride is 1: 40;
[0047] d. Put the mixed liquid C into the hydrothermal reaction kettle and put it in the oven, react at 180℃ for 12 hours to obtain a solid-liquid mixture, pour out the ...
Example Embodiment
[0056] Example 2
[0057] The blue titanium dioxide of this example was prepared as follows:
[0058] a. Dissolve 3 grams of anhydrous titanium tetrachloride in 8ml of absolute ethanol in an ice bath to prepare a titanium tetrachloride ethanol solution with a mass concentration of 32.2%;
[0059] b. At room temperature, add 10ml of titanium trichloride to 25ml of absolute ethanol to obtain mixed solution A, and then add 1.5g of sodium fluoride powder to mixed solution A to obtain mixed solution B. Titanium trichloride and fluoride The molar ratio of sodium powder is 2:1;
[0060] c. At room temperature, add 0.89ml of the ethanol solution of titanium tetrachloride obtained in step a to the mixed solution B obtained in step b to obtain mixed solution C, wherein the molar ratio of titanium tetrachloride to titanium trichloride is 1: 50;
[0061] d. Put the mixed liquid C into a hydrothermal reaction kettle and put it in an oven, and react at a temperature of 180°C for 15 hours to obtain ...
Example Embodiment
[0064] Example 3
[0065] The blue titanium dioxide of this example was prepared as follows:
[0066] a. Dissolve 4 grams of anhydrous titanium tetrachloride in 10ml of absolute ethanol in an ice bath to prepare a titanium tetrachloride ethanol solution with a mass concentration of 33.6%;
[0067] b. At room temperature, add 37.5ml of titanium trichloride to 90ml of absolute ethanol to obtain mixed solution A, and then add 6.5g of sodium fluoride powder to mixed solution A to obtain mixed solution B, titanium trichloride and fluorine The molar ratio of sodium hydroxide powder is 2:1;
[0068] c. At room temperature, add 2.5 ml of the ethanol solution of titanium tetrachloride obtained in step a to the mixed solution B obtained in step b to obtain mixed solution C, wherein the molar ratio of titanium tetrachloride to titanium trichloride is 1: 60;
[0069] d. Put the mixed liquid C into a hydrothermal reaction kettle and put it in an oven, and react at a temperature of 180°C for 15 hou...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap