Devitrification type lead-free low-temperature sealing glass as well as preparation method and application method thereof
A technology for sealing glass and devitrification type, which is applied in the field of devitrification type lead-free low temperature sealing glass, which can solve the problems of not completely solving environmental protection problems, not well satisfied with low temperature sealing and rapid sintering, etc., and achieves low cost and high price. Inexpensive, lower softening temperature effect
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Embodiment 1
[0031] Embodiment 1: Preparation and sealing of materials
[0032] According to the ratio of each component in Table 1, weigh a certain amount of analytically pure raw materials (CaO, SrO, SiO 2 、Al 2 o 3 , B 2 o 3 、 Bi 2 o 3 ), and mixed evenly with a planetary ball mill for 24 hours; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, heat it to 1300°C at 3°C / min, and keep it warm for 1 hour; then, take out the crucible, Pour the melt into deionized water for rapid cooling, and dry to obtain fragments of glass melt; grind and pass through a 100-mesh sieve to obtain glass powder. Mix glass powder with polyvinyl alcohol, fish oil, ethanol and toluene (80%, 2%, 1%, 10%, 7% by weight) to form a slurry, and disperse evenly in a ball mill; tape casting, natural Dry, then cut into the embryo body of the desired shape; place the embryo body at the part to be sealed, heat up at a rate of 2°C / min in an electric furnace,...
Embodiment 2
[0033] Embodiment 2: Preparation and sealing of materials
[0034] According to the ratio of each component in Table 1, weigh a certain amount of analytically pure raw materials (CaO, SrO, SiO 2 、Al 2 o 3 , B 2 o 3 、 Bi 2 o 3 ), use a planetary ball mill for 24 hours to mix evenly; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, heat it at 3°C / min to 1280°C, and keep it warm for 1 hour; then, take out the crucible, Pour the melt into deionized water for rapid cooling, and dry to obtain fragments of glass melt; grind and pass through a 100-mesh sieve to obtain glass powder. Mix glass powder with methylcellulose, polyvinyl alcohol, n-butanol and acetone (82%, 2%, 2%, 8%, 6% by weight) to form a slurry, and disperse evenly in a ball mill; Stretching, drying naturally, and then cutting the embryo body into the desired shape; placing the embryo body on the part to be sealed, raising the temperature in an electric...
Embodiment 3
[0035] Embodiment 3: Preparation and sealing of materials
[0036] According to the ratio of each component in Table 1, weigh a certain amount of analytically pure raw materials (CaO, SrO, SiO 2 、Al 2 o 3 , B 2 o 3 、 Bi 2 o 3 ), use a planetary ball mill for 24 hours to mix evenly; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, heat it at 3°C / min to 1250°C, and keep it warm for 1 hour; then, take out the crucible, Pour the melt into deionized water for rapid cooling, and dry to obtain fragments of glass melt; grind and pass through a 100-mesh sieve to obtain glass powder. Mix glass powder with epoxy resin, polyacrylamide, isopropanol and toluene (84%, 1.5%, 0.5%, 9%, 5% by weight) to form a slurry, and disperse evenly in a ball mill; casting Forming, drying naturally, and then cutting into the embryo body of the desired shape; place the embryo body on the part to be sealed, heat up at a rate of 2°C / min in a...
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